Pt/C催化剂用于硝基苯加氢制备对氨基苯酚的研究
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- 英文论文题名：Catalytic Hydrogenation of Nitrobenzene to p-Aminophenol over Pt/C Catalyst
- 论文作者：王震 ; 周博涵 ; 王丽君
- 英文论文作者：Wang zhen ; Zhou bo han ; Wang li jun ; School of Chemical Engineering ; Anhui University of Science and Technology
- 年：2016
- 作者机构：安徽理工大学化学工程学院;
- 论文关键词：硝基苯 ; 催化加氢 ; Pt/C催化剂 ; 对氨基苯酚
- 英文论文关键词：nitrobenzene ; hydrogenation ; Pt/C catalyst ; p-aminophenol
- 会议召开时间：2016-09-23
- 会议录名称：中部四省化学化工学会2016年学术年会摘要集
- 语种：中文
- 分类号：TQ246.35
- 学会代码：JXHX
- 会议名称：中部四省化学化工学会2016年学术年会
- 会议地点：中国江西南昌
- 主办单位：中国化学会湖北代表处
- 学会名称：江西省化学化工学会
- 页数：1
- 文件大小：108k
- 原文格式：D
- 会议级别：地方
摘要
采用以硝基苯为原料,研究开发以Pt/C为催化剂进行合成路线的选择,介绍了其加氢还原的实验过程及结果讨论,提出对对氨基苯酚生产的一些看法和建议;同时考察了制备条件:浸渍温度、浸渍时间、浸渍液浓度等对Pt/C催化性能的影响。本研究采用常压加氢的工艺路线,考察了反应时间、酸度、助剂、搅拌速度及催化剂用量等工艺参数对反应的转化率和选择性的影响,探讨了在加氢工艺路线中的若干影响因素,如温度、氢分压、PH值及加氢深度等,评述了添加助剂提高对氨基苯酚收率的方法,并对其优缺点进行了讨论。
The performance and application of p-aminophenol were introduced in this article,using nitrobenzene and Pt/C catalyst as raw materials,and the hydrogenation pilot test and the results were also described,Moreover,some comments were put forward on the production of p-aminophenol.Researches in the processes for preparation of p-aminophenol through catalytic hydrogenation of nitrobenzene were reviewed.Influence of some key parameters,such as temperature、partial pressure of hydrogen 、 PH value and hydrogenate on degree were discussed.The advantages and disadvantages of adding promote or to improve the yield of aminophenol were also discussed.
The performance and application of p-aminophenol were introduced in this article,using nitrobenzene and Pt/C catalyst as raw materials,and the hydrogenation pilot test and the results were also described,Moreover,some comments were put forward on the production of p-aminophenol.Researches in the processes for preparation of p-aminophenol through catalytic hydrogenation of nitrobenzene were reviewed.Influence of some key parameters,such as temperature、partial pressure of hydrogen 、 PH value and hydrogenate on degree were discussed.The advantages and disadvantages of adding promote or to improve the yield of aminophenol were also discussed.
引文