离子交换法制备Mn~ⅢTMPyP-LaNb_2O_7纳米复合材料及其电催化性质研究
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- 英文论文题名：Study of Preparing Mn~ⅢTMPyP-LaNb_2O_7 nanocomposite With Ion Exchange Method And Its Electrocatalytic Properties
- 论文作者：许佳晟 ; 张晓波 ; 李金鹏 ; 潘斌斌 ; 童志伟
- 英文论文作者：Jiasheng Xu ; Xiaobo Zhang ; Binbin Pan ; Jinpeng Li ; Zhiwei Tong ; School of Chemical Engineering ; Huaihai Institute of Technology ; School of Chemical Engineering and Technology ; China University of Mining and Technology
- 年：2016
- 作者机构：淮海工学院化学工程学院;中国矿业大学化工学院;
- 论文关键词：插层复合材料 ; 离子交换法 ; 镧铌酸钾 ; 锰卟啉
- 会议召开时间：2016-07-01
- 会议录名称：中国化学会第30届学术年会摘要集-第二十九分会：电化学材料
- 语种：中文
- 分类号：TB33;TB383.1
- 学会代码：ZGHY
- 会议名称：中国化学会第30届学术年会-第二十九分会 ; 电化学材料
- 会议地点：中国辽宁大连
- 主办单位：中国化学会
- 学会名称：中国化学会
- 页数：1
- 文件大小：257k
- 原文格式：D
- 会议级别：全国
摘要
本文以固相合成法制备了主体材料KLaNb_2O_7,并利用二次离子交换法制备了Mn~ⅢTMPyP-LaNb_2O_7纳米复合材料。采用XRD、IR、UV-vis、SEM等方法对获得的纳米复合材料进行表征,并用循环伏安法测试了它的电化学性质。
This paper gives a brief introduction on the preparation of KLaNb_2O_7 host material using high temperature solid phase method, and fabrication of Mn~ⅢTMPyP-LaNb_2O_7 nanocomposite with the secondary ion-exchange method. The structure, morphology and properties of the intercalation compounds are characterized by X-ray diffraction, IR, SEM, UV-vis, etc. The electrochemical behavior of the modified electrodes was investigated by cyclic voltammetry(CV).
This paper gives a brief introduction on the preparation of KLaNb_2O_7 host material using high temperature solid phase method, and fabrication of Mn~ⅢTMPyP-LaNb_2O_7 nanocomposite with the secondary ion-exchange method. The structure, morphology and properties of the intercalation compounds are characterized by X-ray diffraction, IR, SEM, UV-vis, etc. The electrochemical behavior of the modified electrodes was investigated by cyclic voltammetry(CV).
引文
[1]Tong,Z.;Takagi,S.;Shimada,T.;Tachibana,H.;Inoue,H.J.Am.Chem.Soc.2006,128(3),684-685
[2]Ma,J.;Wu,J.;Zheng,J.;Liu,L.;Zhang,D.;Xu,X.;Yang,X.;Tong,Z.Micropor.Mesopor.Mat.2012,151:325-329
[2]Ma,J.;Wu,J.;Zheng,J.;Liu,L.;Zhang,D.;Xu,X.;Yang,X.;Tong,Z.Micropor.Mesopor.Mat.2012,151:325-329