胶原改性剂γ-聚谷氨酸-NHS酯的制备与表征
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- 英文论文题名：The preparation and characterization of the modifier of collagen γ-Poly (glutamic acid)-NHS ester
- 论文作者：杨俊晖 ; 丁翠翠 ; 陈礼辉 ; 黄六莲 ; 张敏
- 英文论文作者：YANG Junhui ; DING Cuicui ; CHENG Lihui ; HUANG Liulian ; ZHANG Min ; College of Materials Engineering ; Fujian Agriculture and Forestry University ; College of Ecological Environment and Urban Construction ; Fujian University of Technology
- 年：2016
- 作者机构：福建农林大学材料工程学院;福建工程学院生态环境与城市建设学院;
- 论文关键词：γ-聚谷氨酸 ; N-羟基琥珀酰亚胺 ; 胶原改性剂
- 英文论文关键词：y-polyglutamic acid ; N-hydroxysuccinimide ester ; modifier of collagen
- 会议召开时间：2016-07-27
- 会议录名称：2016第十一届全国皮革化学品学术交流会暨中国皮革协会技术委员会第21届年会摘要集
- 英文会议录名称：Abstracts of 2016 the 11th National Conference on Leather Chemicals & 21st Annual Convention of China Leather Science and Technology Commission
- 语种：中文
- 分类号：TS529.1
- 学会代码：ZGHG
- 会议名称：2016第十一届全国皮革化学品学术交流会暨中国皮革协会技术委员会第21届年会
- 会议地点：中国山东济南
- 主办单位：中国皮革协会技术委员会、中国皮革协会皮革化工专业委员会、中国化工学会精细化工专业委员会
- 学会名称：中国化工学会
- 页数：1
- 文件大小：48k
- 原文格式：O
- 会议级别：全国
摘要
选用γ-聚谷氨酸(γ-PGA)和N-羟基琥珀酰亚胺(NHS)作为原料,制备胶原改性剂γ-PGA-NHS酯。红外图谱证实γ-PGA-NHS酯具有酯基特征吸收峰,说明γ-PGA-NHS酯制备成功;核磁图谱表明随着NHS加入量的增大,γ-PGA-NHS酯的酯化度也随之增大;差示扫描量热分析说明γ-PGA-NHS酯的热稳定比γ-PGA弱,且酯化度越大,热稳定性越弱。
y-PGA-NHS ester,which was employed as the modifier of collagen,were prepared using y-polyglutamate(y-PGA) and N-hydroxysuccinimide(NHS) as the raw materials.FT-IR was used to characterize the modifier of collagen composition in the prepared y-PGA-NHS ester.The characteristic absorption peak of ester indicated that y-PGA-NHS ester was prepared successfully.Results from nuclear magnetic resonance analysis suggested that the esterification degree of y-PGA-NHS ester increased with the increase of NHS.DSC test were further revealed that the thermal stability of y-PGA-NHS ester was reduced compared with that of pure y-PGA.
y-PGA-NHS ester,which was employed as the modifier of collagen,were prepared using y-polyglutamate(y-PGA) and N-hydroxysuccinimide(NHS) as the raw materials.FT-IR was used to characterize the modifier of collagen composition in the prepared y-PGA-NHS ester.The characteristic absorption peak of ester indicated that y-PGA-NHS ester was prepared successfully.Results from nuclear magnetic resonance analysis suggested that the esterification degree of y-PGA-NHS ester increased with the increase of NHS.DSC test were further revealed that the thermal stability of y-PGA-NHS ester was reduced compared with that of pure y-PGA.
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