气相分子吸收光谱仪光源优化方案探讨
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- 英文论文题名：Discussionof Optimal Light-Source Scheme of GPMAS
- 论文作者：齐文启 ; 臧平安 ; 郝俊 ; 谢东花 ; 刘丰奎 ; 溥旺
- 英文论文作者：Qi Wenqi ; Zang Ping-an ; Hao Jun ; Xie Donghua ; Liu Fengkui ; Pu Wang ; China National Environmental Monitoring Station ; Shanghai Anjie Environmental Protection Technology Co.LTD
- 年：2016
- 作者机构：中国环境监测总站;上海安杰环保科技股份有限公司;
- 论文关键词：气相分子吸收光谱法 ; 氘灯 ; 工作曲线
- 英文论文关键词：Gas Phase Molecular Absorption Spectrometry ; Deuterium Lamp ; Working Curve
- 会议召开时间：2016-09-22
- 会议录名称：2016年中国环境与安全监测技术研讨会—第27届MICONEX2016科学仪器惠及民生系列分会场论文集
- 语种：中文
- 分类号：TH744.12
- 学会代码：XDKX
- 会议名称：2016年中国环境与安全监测技术研讨会—第27届MICONEX2016科学仪器惠及民生系列分会场
- 会议地点：中国北京
- 主办单位：中国仪器仪表学会
- 学会名称：现代科学仪器编辑部
- 页数：3
- 文件大小：2178k
- 原文格式：D
- 会议级别：全国
摘要
气相分子吸收光谱法是在规定的分析条件下,将待测成分转变成气态分子载入测量系统,测定其对特征光谱吸收的方法。最早期的气相分子吸收光谱仪是经过原子吸收光谱仪改装的,所以光源采用空心阴极灯。本文对光源的优化做了探讨。通过一系列对比实验得出结论,应用氘灯做光源更加准确合理。改进后的气相分子吸收光谱仪,所做工作曲线线性良好,测量结果完全满足环保标准方法的要求,同时单一光源操作更加方便。
Gas Phase Molecular Absorption Spectrometry is that the detected substance is inverted into gas molecules to be loaded in a measuring system under the specified analytical conditions.Gas Phase Molecular Absorption Spectrometer was modified by Atomic Absorption Spectrometer in the early times, socathode lampwas used by the light source. In this thesis, it mainly is discussedto set up optimal mode of light source.Through a series of comparative experiments,it provedthat deuterium lampwasusedfor light sourcewhichwasmore accurate and reasonable. Afterbeingimprovedgas phase molecular absorption spectrometer, satisfactorylinearityofworkingcurvewas obtained.Measurement results completely satisfied the requirements of standard methodfor environmental protection, at the same time, it is convenientto operate single-light.
Gas Phase Molecular Absorption Spectrometry is that the detected substance is inverted into gas molecules to be loaded in a measuring system under the specified analytical conditions.Gas Phase Molecular Absorption Spectrometer was modified by Atomic Absorption Spectrometer in the early times, socathode lampwas used by the light source. In this thesis, it mainly is discussedto set up optimal mode of light source.Through a series of comparative experiments,it provedthat deuterium lampwasusedfor light sourcewhichwasmore accurate and reasonable. Afterbeingimprovedgas phase molecular absorption spectrometer, satisfactorylinearityofworkingcurvewas obtained.Measurement results completely satisfied the requirements of standard methodfor environmental protection, at the same time, it is convenientto operate single-light.
引文
[1]HJ/T 198-2005水质硝酸盐氮的测定气相分子吸收光谱法[S].
[2]臧平安,气相分子吸收光谱法测定硝酸盐氮的研究[J],宝钢技术,1995,24-30
[3]吴卓智,莫怡玉,吴银笑,陈羽波,气相分子吸收光谱法测定硝酸盐氮的改进方法[J].现代仪器,2003,(5):23-24,32.
[2]臧平安,气相分子吸收光谱法测定硝酸盐氮的研究[J],宝钢技术,1995,24-30
[3]吴卓智,莫怡玉,吴银笑,陈羽波,气相分子吸收光谱法测定硝酸盐氮的改进方法[J].现代仪器,2003,(5):23-24,32.