密胺树脂薰衣草精油微胶囊的制备
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- 英文论文题名：Preparation of Melamine Resin Incense Lavender Essential Oil Microcapsules
- 论文作者：宋晓秋 ; 段玉萍 ; 叶琳
- 英文论文作者：Song Xiaoqiu ; Duan Yuping ; Ye Lin ; Shanghai Institute of Technology School of Perfume and Aroma Technology
- 年：2016
- 作者机构：上海应用技术大学香料香精技术与工程学院;
- 论文关键词：薰衣草精油 ; 密胺树脂 ; 微胶囊 ; 原位聚合法
- 英文论文关键词：lavender essential oil ; melamine resin ; microcapsule ; in-situ polymerization
- 会议召开时间：2016-06-15
- 会议录名称：第十一届中国香料香精学术研讨会论文集
- 英文会议录名称：The Proceedings of the 11th Seminar on Fragrance and Flavor China
- 语种：中文
- 分类号：TQ654.2
- 学会代码：ZGXE
- 会议名称：第十一届中国香料香精学术研讨会
- 会议地点：中国上海
- 主办单位：中国香料香精化妆品工业协会
- 学会名称：中国香料香精化妆品工业协会
- 页数：6
- 文件大小：666k
- 原文格式：O
- 会议级别：全国
摘要
以薰衣草精油为芯材,密胺树脂为壁材,采用原位聚合法制备了密胺树脂薰衣草精油微胶囊。通过扫描电镜(SEM),紫外可见分光光度计和热重分析仪(TGA)等仪器对其进行检测表征。结果表明,当制备工艺为乳化剂SMANa、SDS与司班-80三种乳化剂复配,加入量占芯材质量分数的5%,芯材壁材质量比为1:1,搅拌速度为1100rpm时,所制备的微胶囊整体性能最好。SEM电镜照片表明,微胶囊为球形,粒径1-4μm且分布均匀,表面较光滑且无孔洞、裂缝存在;紫外可见分光光度计测得,该微胶囊为全封闭型薰衣草精油微胶裳。
The melamine resin lavender essential oil microcapsules were prepared by in-situ polymerization with melamine resin as outer shell and lavender essential oil as core material.Microcapsules were characterized by scanning electron microscopy(SEM),UV spectrophotometer and thermal gravimetric analysis(TGA),ea tl.The results show that the best conditions for preparation of melamine resin lavender essential oil microcapsules are:using SMANa,SDS and s-80 as complex emulsifier,5%to lavender essential oil,the core/shell mass ratio is 1:1,stirring speed is 1100 rpm.The SEM show that the average particle size of melamine resin lavender essential oil microcapsules is l-4μm,the surface is smooth and has no holes and cracks.The UV result show that the microcapsules are all closed lavender essential oil microcapsules.
The melamine resin lavender essential oil microcapsules were prepared by in-situ polymerization with melamine resin as outer shell and lavender essential oil as core material.Microcapsules were characterized by scanning electron microscopy(SEM),UV spectrophotometer and thermal gravimetric analysis(TGA),ea tl.The results show that the best conditions for preparation of melamine resin lavender essential oil microcapsules are:using SMANa,SDS and s-80 as complex emulsifier,5%to lavender essential oil,the core/shell mass ratio is 1:1,stirring speed is 1100 rpm.The SEM show that the average particle size of melamine resin lavender essential oil microcapsules is l-4μm,the surface is smooth and has no holes and cracks.The UV result show that the microcapsules are all closed lavender essential oil microcapsules.
引文
[1]李玉赜,赵艳.玫瑰花的营养价值与保健功能.中国食物与营养,2008,12(4):54—55.
[2]李明,李艳芳,孙永超.中药玫瑰花的研究进展.卫生职业教育,2007,25(8):146-148.
[3]Martin Del.Valle E M.Cyclodextrins and their uses.Process Biochemistry,2004,39:1033-1046.
[4]董桂蕃,姜晓舜,董言德,等.吸血昆虫的化学防护北京:军事医学科学出版社,1999.
[5]欧阳杰,王晓东,赵兵,等.香料植物应用研究进展.香料香精化妆品,2002,5:32-34.
[6]Craig B,Warren Jerry F,Marin Anna B,Butler.Use of unsaturated aldehyde and alkanol derivatives for their mosquito repellency propertiesUSA,Chemistry,5665781,1997.
[7]Dotolo VincentPesticides containing D-limonene USA,Chemistry,4379168,1983.
[8]Rodrigues S N,Martins I M.Microencapsulated perfumes for textile application.Chemical Engineering Journal,2009,149:463-472.
[9]Zhang X,Fan Y,Tao X,et al.Fabrication and properties of microcapsules and nanocapsules containing n-octadecane.Mater Chem Phys,2004,88:300.
[10]Zhang H Z,Sun S Y,Wang X D,et al.Fabrication of microencapsulated phase change materials based on n-octadecanecore and silica shell through interfacial polycondensation.Colloids Surf A:Physicochem,2011,38:104-117.
[11]Benita S.Microencapsulation:methods and industrial applications.New York:Marcel Dekker,1996:1-20.
[12]Badulescu,V.Vivod,DJausovec,B-Voncina.Treatment of CottonFabrics-with Ethyl Cellulose Microcapsules.Medical and Healthcare Textiles.2010,8:226-235.
[13]Zhijian Dong,Yong Ma,Khizar Hayat,et al.Morphology and release profile of microcapsules encapsulating peppermint oil by complex coacervation.Journal of Food Engineering.2011,104:455-460.
[14]Kuan-Wen Yeh.Chih Pong Chang,Takao Yamamoto,et al.Release model of alginate microcapsules containing volatile tea-tree oil.Colloids and Surfaces A:Physicochemical and Engineering Aspects.2011,308:152-155.
[15]Yang Hu,Yu Yang,Yin Ning,et al.Facile preparation of artemisia argyi oil-loaded antibacterial microcapsules by hydroxyapatite-stabili2ed Pickering emulsion templating.Colloids and Surfaces B:Biointerfaces.2013,112:96-102.
[16]Pablo Monllor,Maria Angeles Bonet,Francisco Cases.Characterization of the behaviour of flavour microcapsules in cotton fabrics.European Polymer Journal.2007,43:2481-2490.
[17]Brisa Pena,Cinta Panisello,Gemma Aresté,et al.Preparation and characterization of polysulfone microcapsules for perfume release.Chemical Engineering Journal.2012,79:394-403.
[2]李明,李艳芳,孙永超.中药玫瑰花的研究进展.卫生职业教育,2007,25(8):146-148.
[3]Martin Del.Valle E M.Cyclodextrins and their uses.Process Biochemistry,2004,39:1033-1046.
[4]董桂蕃,姜晓舜,董言德,等.吸血昆虫的化学防护北京:军事医学科学出版社,1999.
[5]欧阳杰,王晓东,赵兵,等.香料植物应用研究进展.香料香精化妆品,2002,5:32-34.
[6]Craig B,Warren Jerry F,Marin Anna B,Butler.Use of unsaturated aldehyde and alkanol derivatives for their mosquito repellency propertiesUSA,Chemistry,5665781,1997.
[7]Dotolo VincentPesticides containing D-limonene USA,Chemistry,4379168,1983.
[8]Rodrigues S N,Martins I M.Microencapsulated perfumes for textile application.Chemical Engineering Journal,2009,149:463-472.
[9]Zhang X,Fan Y,Tao X,et al.Fabrication and properties of microcapsules and nanocapsules containing n-octadecane.Mater Chem Phys,2004,88:300.
[10]Zhang H Z,Sun S Y,Wang X D,et al.Fabrication of microencapsulated phase change materials based on n-octadecanecore and silica shell through interfacial polycondensation.Colloids Surf A:Physicochem,2011,38:104-117.
[11]Benita S.Microencapsulation:methods and industrial applications.New York:Marcel Dekker,1996:1-20.
[12]Badulescu,V.Vivod,DJausovec,B-Voncina.Treatment of CottonFabrics-with Ethyl Cellulose Microcapsules.Medical and Healthcare Textiles.2010,8:226-235.
[13]Zhijian Dong,Yong Ma,Khizar Hayat,et al.Morphology and release profile of microcapsules encapsulating peppermint oil by complex coacervation.Journal of Food Engineering.2011,104:455-460.
[14]Kuan-Wen Yeh.Chih Pong Chang,Takao Yamamoto,et al.Release model of alginate microcapsules containing volatile tea-tree oil.Colloids and Surfaces A:Physicochemical and Engineering Aspects.2011,308:152-155.
[15]Yang Hu,Yu Yang,Yin Ning,et al.Facile preparation of artemisia argyi oil-loaded antibacterial microcapsules by hydroxyapatite-stabili2ed Pickering emulsion templating.Colloids and Surfaces B:Biointerfaces.2013,112:96-102.
[16]Pablo Monllor,Maria Angeles Bonet,Francisco Cases.Characterization of the behaviour of flavour microcapsules in cotton fabrics.European Polymer Journal.2007,43:2481-2490.
[17]Brisa Pena,Cinta Panisello,Gemma Aresté,et al.Preparation and characterization of polysulfone microcapsules for perfume release.Chemical Engineering Journal.2012,79:394-403.