油页岩废渣膏体充填材料研究
摘要
膏体充填开采是当代煤炭工业实现不迁址开采，解决三下采煤、提高煤炭采出率的最有效的一种途径。本文主要对油页岩废渣制备矿山膏体充填材料及泵送工艺进行研究。此项技术不仅充分利用了废弃资源，还有效的保护了农田、村庄、河流、建筑等等，降低了煤矿开采的成本，提高了煤炭资源开采率，近年来国内已有数家煤炭企业试图运用推广此项技术，但是对于使用油页岩废渣在膏体充填中的实际制备和性能还没有系统研究而未能产业化。本文对利用油页岩废渣制备膏体充填材料的制备进行了一系列的研究分析，对页岩废渣作为膏体充填材料中的胶凝材料做了细致的实验，对膏体充填工艺进行了探讨，对膏体充填材料的性能指标检测及微观形态进行分析。
Mining with paste filling is a contemporary coal industryimplementation does not move mining, coal mining under three, toimprove coal mining rate of one of the most effective ways. This paperfocuses on the oil shale residue for preparing mine paste filling materialand pumping technology research. This technique not only makes full useof waste resource, but also effectively protect the farmland, villages,rivers, buildings and so on, reduce the cost of mining, improve coalmining rate, in recent years the domestic several coal company tries topopularize this technology, but for the use of oil shale residue in pastefilling the actual preparation and performance has not been studiedsystematically to industrialization. This article on the use of oil shalewaste preparation of paste filling material preparation conducted a seriesof research and analysis, on shale residue as a filling material incementitious materials made of detailed experiments, the paste fillingtechnology was discussed, the paste filling material performancedetection and morphology of analysis of.
Mining with paste filling is a contemporary coal industryimplementation does not move mining, coal mining under three, toimprove coal mining rate of one of the most effective ways. This paperfocuses on the oil shale residue for preparing mine paste filling materialand pumping technology research. This technique not only makes full useof waste resource, but also effectively protect the farmland, villages,rivers, buildings and so on, reduce the cost of mining, improve coalmining rate, in recent years the domestic several coal company tries topopularize this technology, but for the use of oil shale residue in pastefilling the actual preparation and performance has not been studiedsystematically to industrialization. This article on the use of oil shalewaste preparation of paste filling material preparation conducted a seriesof research and analysis, on shale residue as a filling material incementitious materials made of detailed experiments, the paste fillingtechnology was discussed, the paste filling material performancedetection and morphology of analysis of.
引文
[1] Bakharev, T., Sanjayan, J.G.andeCheng.Y.B.,2001a, Resistance of alkali-activatedslag concrete to alkali-aggregate reaction.Cement and Concrete Researcb,31(2),331-334.
[2] Bakharev, T., Sanjayan, J.G.andeCheng.Y.B.,2001b, Resistance of alkali-activatedslag concrete to carbonation reaction. Cement and Concrete Researcb,31(9),1277-1283.
[3] Bakharev, T., Sanjayan, J.G.andeCheng.Y.B.,2002, Sulphate attack onalkaliactivated slag concrete.Cement and Concrete Researcb,31(9),1277-1283.
[4] Collins,F.G. and Sanjayan,J.G.,2000a,Cracking tendency of alkali-activated slagconcrete subjected to restrained shrinkage.Cement and ConcreteResearch,30(5),791-798.
[5] Collins,F.G. and Sanjayan,J.G.,2000b,Effect of pore size distribution on dryingshrinkage of alkali-activated slag concrete.Cement and ConcreteResearch,30(9),1401-1406.
[6] Collins,F.G. and Sanjayan,J.G.,2001a,Early age strength and workability sodiumsilicates.Magazine of Concrete Research,52(5)321-326.
[7] Davidovits,J.1991.Geopolymers:inorganic polymeric new materials.ThermalAnalysia.37:1633-1656.
[8] Mehta,P.K,”Reducing the Environmental Impact of Concrete”.ConcreteInternational,2001,23(3)25-34.
[9] Davidovits,J.The Anicient Egyptian Pyramids-Concrete or Rock[J].ConcreteInternational,1987,9(12):28-32.
[10] Garrett,D.E.,1992,Natural Soda Ash-Occurrences,Processing and Use(NewYork:Van Nostrand Reinhold).
[11] Geiseler,J.;1996,Use of steel works slag in Europe.WasteManagement,16(1-3),59-63.
[12] Hong,S.Y.and Glasser,F.P.;1999,Alkali binding in cement pastes.Cement andConcrete Research,29(12),1893-1904.
[13] Hogan,F.J.,1983,Study of grinding energy required for pelleteized and watergranulated slag.Silicates Industriels,3,71-78.
[14]Hogan,F.J.,1985,The effect of blast furnace slag cement on alkali-aggregatereactivity:A literature review.Cement,Concrete,and Aggregate,7(2),100-107.
[15]侯云芬，王栋民，李俏.激发剂对粉煤灰基地质聚合物抗压强度的影响[J].建筑材料学报.2007，10(2):99-103.
[16]徐树岚,苏家宏.充填采矿法[C].长沙：中国金属学会采矿学术委员会.1999.21-26.
[17]丰裕军.下向分层胶结充填采矿法在我国岩金地下矿山的应用与发展[J].黄金,2000,(1):17-18.
[18]马英芳编著，现代充填基础理论[M].，西安：西安冶金建筑学院，1988.4.
[19]侯云芬，王栋民，李俏.水玻璃性能对粉煤灰基矿物聚合物的影响[J].硅酸盐学报2008，1：62-68.
[20]王致清主编.粘性流体动力学[M]，哈尔滨：哈尔滨工业大学出版社，1990.
[21]长沙矿山研究院,长沙有色冶金设计研究院,长沙矿冶研究所,等.充填采矿法
[M].北京:冶金工业出版社,1978.
[22]蔡嗣经编著，矿山充填力学基础[M]，北京：冶金工业出版社，1994.6.
[23]郑娟荣，谭维祖.地聚物材料的研究进展[J].新型建筑材料.2002，4:11-12.
[24]刘同有,周成浦,金铭良,等.充填采矿技术与应用[M].北京:冶金工业出版社,2001.
[25]蔡嗣经.充填采矿法的新理论、新工艺和新方案[A].第二届冶金矿山采矿技术进展报告会论文集[C].成都:全国冶金矿山信息网,1991.86-87.
[26]王正辉.膏休充填料的工程检测与判别[J]，有色矿山，2000.5.15-17
[27]黄志伟.无废开采评价理论的研究[M].长沙:中南大学出版社,2003.
[28]周成浦.流态混凝土与全尾砂膏体充填料[J]，有色矿山，1996.11.19-20
[29]周成浦等.金川胶结充填技术新进展[J]，有色矿山，1992.4
[30]徐树岚,苏家宏.充填采矿法[C].长沙:中国金属学会采矿学术委员会.1999.21-22.
[31]张冠伦等编著.混凝土外加剂原理与应用[M].北京：中国建筑工业出版社，1987.5
[32]王佩勋，王五松.充填料浆输送管道磨损规律分析[A]，第二届中日浆体输送技术交流会论文集[C]，1998.10
[33]周成浦，浆体充填与高体充填技术对比与分析，金川科技，1998.8
[34]冶金部长沙矿山研究院编.充填采矿法[M].北京：冶金工业出版社，1978.9
[35]丁宏达等著.浆体管道输送原理和工程系统设计[M]，中国金属学会浆体输送学术委员会，1990.5
[36]王立刚，朱曦光.我国粉煤灰资源的综合利用现状及今后发展重点[J].矿业研究与开发,1995,(5):16-17.
[37]米家纸.计算流体力学[M]，北京：科学出版社，1985.8
[38]赵学端.廖其鉴.粘性流体力学[M]，北京：机械工业出版社，1983.6
[39]于学馥，刘同有.金川的充填机理与采矿理论[A]，面向21世纪的岩石力学与工程：中国岩石力学与工程学会第四次学术大会论文集[C]，1996.
[40]林国洪，张葆春，周建华.全尾砂高水固化材料下向充填采矿法的应用[J]，有色矿山，2000.4.
[41]王绍周等著，粒状物料的浆体管道输送[M]，北京：海洋出版社，1998.1
[42]孙恒虎黄玉诚杨宝贵编著，当代胶结充填技术[M]，北京：冶金工业出版社，2002
[43]郑娟荣，刘丽娜.偏高岭土基地质聚合物合成条件的试验研究[J].郑州大学学报2008，6.44-47
[44]侯云芬，王栋民，李俏.粉煤灰基地质聚合物的试验研究[J].粉煤灰综合利用2007，4:35-38
[45]周爱民矿山废料交结充填[M].北京：冶金工业出版社2007，
[46]蔡嗣经矿山充填力学基础[M].北京：冶金工业出版社2009，
[47]刘同有等编著，充填采矿技术与应用[M]，北京：冶金工业出版社，2001
[48]章梓雄董曾南，粘性流体力学[M]，北京：清华大学出版社，1998
[49]彭继承主编，充填理论及应用[M]，长沙：中南工业大学出版社，1998.2
[50]霍米亚科夫著，国外矿山充填经验[M]，长沙：长沙矿山研究院管道输送研究室译1989.5
[2] Bakharev, T., Sanjayan, J.G.andeCheng.Y.B.,2001b, Resistance of alkali-activatedslag concrete to carbonation reaction. Cement and Concrete Researcb,31(9),1277-1283.
[3] Bakharev, T., Sanjayan, J.G.andeCheng.Y.B.,2002, Sulphate attack onalkaliactivated slag concrete.Cement and Concrete Researcb,31(9),1277-1283.
[4] Collins,F.G. and Sanjayan,J.G.,2000a,Cracking tendency of alkali-activated slagconcrete subjected to restrained shrinkage.Cement and ConcreteResearch,30(5),791-798.
[5] Collins,F.G. and Sanjayan,J.G.,2000b,Effect of pore size distribution on dryingshrinkage of alkali-activated slag concrete.Cement and ConcreteResearch,30(9),1401-1406.
[6] Collins,F.G. and Sanjayan,J.G.,2001a,Early age strength and workability sodiumsilicates.Magazine of Concrete Research,52(5)321-326.
[7] Davidovits,J.1991.Geopolymers:inorganic polymeric new materials.ThermalAnalysia.37:1633-1656.
[8] Mehta,P.K,”Reducing the Environmental Impact of Concrete”.ConcreteInternational,2001,23(3)25-34.
[9] Davidovits,J.The Anicient Egyptian Pyramids-Concrete or Rock[J].ConcreteInternational,1987,9(12):28-32.
[10] Garrett,D.E.,1992,Natural Soda Ash-Occurrences,Processing and Use(NewYork:Van Nostrand Reinhold).
[11] Geiseler,J.;1996,Use of steel works slag in Europe.WasteManagement,16(1-3),59-63.
[12] Hong,S.Y.and Glasser,F.P.;1999,Alkali binding in cement pastes.Cement andConcrete Research,29(12),1893-1904.
[13] Hogan,F.J.,1983,Study of grinding energy required for pelleteized and watergranulated slag.Silicates Industriels,3,71-78.
[14]Hogan,F.J.,1985,The effect of blast furnace slag cement on alkali-aggregatereactivity:A literature review.Cement,Concrete,and Aggregate,7(2),100-107.
[15]侯云芬，王栋民，李俏.激发剂对粉煤灰基地质聚合物抗压强度的影响[J].建筑材料学报.2007，10(2):99-103.
[16]徐树岚,苏家宏.充填采矿法[C].长沙：中国金属学会采矿学术委员会.1999.21-26.
[17]丰裕军.下向分层胶结充填采矿法在我国岩金地下矿山的应用与发展[J].黄金,2000,(1):17-18.
[18]马英芳编著，现代充填基础理论[M].，西安：西安冶金建筑学院，1988.4.
[19]侯云芬，王栋民，李俏.水玻璃性能对粉煤灰基矿物聚合物的影响[J].硅酸盐学报2008，1：62-68.
[20]王致清主编.粘性流体动力学[M]，哈尔滨：哈尔滨工业大学出版社，1990.
[21]长沙矿山研究院,长沙有色冶金设计研究院,长沙矿冶研究所,等.充填采矿法
[M].北京:冶金工业出版社,1978.
[22]蔡嗣经编著，矿山充填力学基础[M]，北京：冶金工业出版社，1994.6.
[23]郑娟荣，谭维祖.地聚物材料的研究进展[J].新型建筑材料.2002，4:11-12.
[24]刘同有,周成浦,金铭良,等.充填采矿技术与应用[M].北京:冶金工业出版社,2001.
[25]蔡嗣经.充填采矿法的新理论、新工艺和新方案[A].第二届冶金矿山采矿技术进展报告会论文集[C].成都:全国冶金矿山信息网,1991.86-87.
[26]王正辉.膏休充填料的工程检测与判别[J]，有色矿山，2000.5.15-17
[27]黄志伟.无废开采评价理论的研究[M].长沙:中南大学出版社,2003.
[28]周成浦.流态混凝土与全尾砂膏体充填料[J]，有色矿山，1996.11.19-20
[29]周成浦等.金川胶结充填技术新进展[J]，有色矿山，1992.4
[30]徐树岚,苏家宏.充填采矿法[C].长沙:中国金属学会采矿学术委员会.1999.21-22.
[31]张冠伦等编著.混凝土外加剂原理与应用[M].北京：中国建筑工业出版社，1987.5
[32]王佩勋，王五松.充填料浆输送管道磨损规律分析[A]，第二届中日浆体输送技术交流会论文集[C]，1998.10
[33]周成浦，浆体充填与高体充填技术对比与分析，金川科技，1998.8
[34]冶金部长沙矿山研究院编.充填采矿法[M].北京：冶金工业出版社，1978.9
[35]丁宏达等著.浆体管道输送原理和工程系统设计[M]，中国金属学会浆体输送学术委员会，1990.5
[36]王立刚，朱曦光.我国粉煤灰资源的综合利用现状及今后发展重点[J].矿业研究与开发,1995,(5):16-17.
[37]米家纸.计算流体力学[M]，北京：科学出版社，1985.8
[38]赵学端.廖其鉴.粘性流体力学[M]，北京：机械工业出版社，1983.6
[39]于学馥，刘同有.金川的充填机理与采矿理论[A]，面向21世纪的岩石力学与工程：中国岩石力学与工程学会第四次学术大会论文集[C]，1996.
[40]林国洪，张葆春，周建华.全尾砂高水固化材料下向充填采矿法的应用[J]，有色矿山，2000.4.
[41]王绍周等著，粒状物料的浆体管道输送[M]，北京：海洋出版社，1998.1
[42]孙恒虎黄玉诚杨宝贵编著，当代胶结充填技术[M]，北京：冶金工业出版社，2002
[43]郑娟荣，刘丽娜.偏高岭土基地质聚合物合成条件的试验研究[J].郑州大学学报2008，6.44-47
[44]侯云芬，王栋民，李俏.粉煤灰基地质聚合物的试验研究[J].粉煤灰综合利用2007，4:35-38
[45]周爱民矿山废料交结充填[M].北京：冶金工业出版社2007，
[46]蔡嗣经矿山充填力学基础[M].北京：冶金工业出版社2009，
[47]刘同有等编著，充填采矿技术与应用[M]，北京：冶金工业出版社，2001
[48]章梓雄董曾南，粘性流体力学[M]，北京：清华大学出版社，1998
[49]彭继承主编，充填理论及应用[M]，长沙：中南工业大学出版社，1998.2
[50]霍米亚科夫著，国外矿山充填经验[M]，长沙：长沙矿山研究院管道输送研究室译1989.5