激光法连续制备荧光性的修饰纳米氧化锌有机溶胶及其PS杂化材料
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摘要
采用聚焦脉冲激光束轰击浸于含修饰剂流动液相中的氧化物固体靶的连续一步制备的新方法,将杂化材料的制备、原位修饰、组装和杂化一步连续完成,获得修饰性纳米氧化物乙醇溶胶和修饰性纳米氧化物/聚合物杂化溶胶,进而获得聚合物杂化薄膜材料,发现该聚合物杂化薄膜材料具有强的荧光特性,可在光致电致发光和LED上具有潜在的应用前景。
本论文采用聚焦脉冲激光束轰击浸于含修饰剂流动液相中的ZnO固体靶,连续制备得到修饰纳米ZnO乙醇溶胶,修饰纳米ZnO/PS有机溶胶并由此获得修饰纳米ZnO/PS杂化薄膜。研究发现ZnO乙醇溶胶和杂化薄膜在紫外光的照射下能发射强的蓝光;ZnO的粒径分布为15～30 nm;ZnO/PS杂化薄膜的热稳定性较纯的PS薄膜有所提高。
采用脉冲激光法分别制备得到发蓝光的修饰纳米ZnO有机溶胶、发绿光的修饰纳米Al_2O_3有机溶胶和发红光的修饰纳米Eu_2O_3有机溶胶,溶胶以一定的比例混合,得到修饰纳米氧化物混合有机溶胶,并由此获得修饰纳米氧化物/PS杂化薄膜。通过UV-Vis、TEM、TG-DSC、荧光光谱等对修饰纳米氧化物混合有机溶胶和修饰纳米氧化物/PS杂化薄膜的结构、基本性质和荧光特性进行表征,发现在一定波长的紫外光的激发下,混合有机溶胶和杂化薄膜能产生混合白光。
The preparation of hybrid material,decoration in situ,assembly and hybrid are one-step continuously completed by pulsed laser ablation.Decorated nano-oxide ethanol sols and decorated nano-oxide/polymer organic sols are successively produced by pulsed laser ablation at the interface of oxide target submerged in the flowing liquid which contained modification agents.Then decorated nano-oxide/polymer hybrid thin films are obtained.It is found that the nano-oxide/polymer hybrid thin films radiate high fluorescence,which may be applied in LED in future.
In this paper,decorated nano-ZnO ethanol sols and decorated nano ZnO/PS organic sols which were modified in situ were successively produced by pulsed laser ablation at the interface of ZnO target submerged in the flowing liquid which contained modification agents.Then decorated nano ZnO/PS hybrid thin films were obtained.It was found that Decorated nano-ZnO ethanol sols and decorated nano ZnO/PS hybrid thin films radiated intense blue light under ultraviolet radiation.TEM showed that the size of the nano ZnO particles distributed between 15 nm and 30 nm.TG-DSC revealed that the heat resistance of decorated nano ZnO/PS hybrid thin flims increased.
Decorated nano-ZnO organic sols,decorated nano-Al_2O_3 organic sols and decorated nano-Eu_2O_3 organic sols were successively produced by pulsed laser ablation.Decorated nano-oxide mixed organic sols were obtained by mixing the three sols,then decorated nano-oxide/PS hybrid thin films were produced.The organic sols and hybrid thin films were investigated by TEM,UV-Vis,TG-DSC and fluorescence spectrum.It was found that the organic sols and hybrid thin films can radiate white light under ultraviolet radiation.
本论文采用聚焦脉冲激光束轰击浸于含修饰剂流动液相中的ZnO固体靶,连续制备得到修饰纳米ZnO乙醇溶胶,修饰纳米ZnO/PS有机溶胶并由此获得修饰纳米ZnO/PS杂化薄膜。研究发现ZnO乙醇溶胶和杂化薄膜在紫外光的照射下能发射强的蓝光;ZnO的粒径分布为15～30 nm;ZnO/PS杂化薄膜的热稳定性较纯的PS薄膜有所提高。
采用脉冲激光法分别制备得到发蓝光的修饰纳米ZnO有机溶胶、发绿光的修饰纳米Al_2O_3有机溶胶和发红光的修饰纳米Eu_2O_3有机溶胶,溶胶以一定的比例混合,得到修饰纳米氧化物混合有机溶胶,并由此获得修饰纳米氧化物/PS杂化薄膜。通过UV-Vis、TEM、TG-DSC、荧光光谱等对修饰纳米氧化物混合有机溶胶和修饰纳米氧化物/PS杂化薄膜的结构、基本性质和荧光特性进行表征,发现在一定波长的紫外光的激发下,混合有机溶胶和杂化薄膜能产生混合白光。
The preparation of hybrid material,decoration in situ,assembly and hybrid are one-step continuously completed by pulsed laser ablation.Decorated nano-oxide ethanol sols and decorated nano-oxide/polymer organic sols are successively produced by pulsed laser ablation at the interface of oxide target submerged in the flowing liquid which contained modification agents.Then decorated nano-oxide/polymer hybrid thin films are obtained.It is found that the nano-oxide/polymer hybrid thin films radiate high fluorescence,which may be applied in LED in future.
In this paper,decorated nano-ZnO ethanol sols and decorated nano ZnO/PS organic sols which were modified in situ were successively produced by pulsed laser ablation at the interface of ZnO target submerged in the flowing liquid which contained modification agents.Then decorated nano ZnO/PS hybrid thin films were obtained.It was found that Decorated nano-ZnO ethanol sols and decorated nano ZnO/PS hybrid thin films radiated intense blue light under ultraviolet radiation.TEM showed that the size of the nano ZnO particles distributed between 15 nm and 30 nm.TG-DSC revealed that the heat resistance of decorated nano ZnO/PS hybrid thin flims increased.
Decorated nano-ZnO organic sols,decorated nano-Al_2O_3 organic sols and decorated nano-Eu_2O_3 organic sols were successively produced by pulsed laser ablation.Decorated nano-oxide mixed organic sols were obtained by mixing the three sols,then decorated nano-oxide/PS hybrid thin films were produced.The organic sols and hybrid thin films were investigated by TEM,UV-Vis,TG-DSC and fluorescence spectrum.It was found that the organic sols and hybrid thin films can radiate white light under ultraviolet radiation.
引文
[1]Bagnall D.M.,Chen Y.F.,Zhu Z.,et al..Optical pumped lasing of ZnO at room temperature[J].Appl Phys Lett,1997,70(17):2230-2232
[2]Zu P.,Tang Z.K.,Kawasaki M.,et al..Ultraviolet spontaneous and stimulated emission from ZnO micro crystalline thin films at room temperature[J].Solid State Com,1997,103(8):459-463
[3]Du Y.,Zang M.S.,Hong J.,et al..Structural and optical properties of nanophase zinc oxide[J].Applied Physics A.2003,76:171-176
[4]Dierstein A.,Natter H.,Meyer F.,et al..Electrochemical deposition under oxidizing conditions (EDOC):a new synthesis for nanocrystalline metal oxides[J].Scripta mater,2001,44(8/9):2209-2212
[5]Posner E.G..Colloidal zinc oxide[P].US24359,1995,9(14)
[6]朱勇,沈辉,刘佩田,等.激光加热制备ZnO纳米粉[J].无机材料学报,1993,8(1):111-113
[7]Thangaraju B..Structural and electrical studies on highly conducting spray deposited fluorine and antimony doped SnO_2 thin films from SnCl_2 precursor[J].Thin Solid Films,2002,402(1-2):71-78
[8]赵新宇,郑柏存,李春中,等.喷雾热解合成ZnO超细粒子工艺及机理研究[J].无机材料学报,1996,11(4):611-616
[9]俞建群,贾殿赠,郑毓锋,等.纳米氧化镍,氧化锌的合成新方法[J].无机化学学报,1999,15(1):95-98
[10]沈茹娟,贾殿赠,梁凯,等.纳米氧化锌的固相合成及其气敏特性[J].无机化学学报,2000,16(6):906-910
[11]Takuya T.,Paul G M..ZnO nanoparticles synthesised by mechanochemical processing[J].Scripta mater,2001,44(8/9):1731-1734
[12]黄志明,刘建斌,许民.纳米氧化锌的固相合成[J].有色金属,2004(1):41-43
[13]亓秀芹,陶栋梁,黄毅,等.氧化锌纳米棒的生长过程研究[J].光谱学与光谱分析,2005,25(3):321-325
[14]张士成,李春和,李星.纳米氧化锌的粒度控制与表征[J].物理化学学报,2004,20(8):902-905
[15]罗志强,张孝彬,程继鹏,等.化学溶液沉积法制备单分散氧化锌纳米棒阵列[J].化学学报,2005,63(18):1656-1660
[16]杨青林,郭林,吴中华,等.室温下纳米氧化锌新相的合成及表征[J].高等化学学报,2003(24):82-85
[17]徐甲强,潘庆谊,孙雨安,等.纳米氧化锌的乳液合成,结构表征与气敏性能[J].无机化学学报,1998,14(3):355-359
[18]Yu B.L.,Zou B.S.,Wu X.C..Preparation of ZnO nanometer powder and their ESR properties [J].Chinese Journal of Semiconductors,1995,16(7):558-560
[19]Daisuke K.,Hideki S.,Takeshi K.,et al..Synthesis of ZnO particles by ammonia-catalyzed hydrolysis of Zinc dibutoxide in nonionic reversed micelles[J].Langmuir,2000,16(9):4086-4089
[20]陈友存,张元广,周根.棒状和球状氧化锌微晶的控制合成及其表征[J].无机材料学报,2004,19(5):1173-1176
[21]李汶军,施尔畏,王步国,等.水热法制备氧化锌粉体[J].无机材料学报,1998,13(1):27-32
[22]徐甲强,纪朋,李志伟,等.水热法合成氧化锌亚微米棒及气敏性能研究[J].郑州轻工业学院学报(自然科学版),2005,20(3):1-3
[23]郭敏,刁鹏,蔡生民.水热法制备高度取向的氧化锌纳米棒阵列[J].高等学校化学学报,2004,2(2):345-347
[24]宋旭春,徐铸德,陈卫祥,等.氧化锌纳米棒的制备和生长机理研究[J].无机化学学报,2004,20(2):186-190
[25]刘雪宁,杨治中,唐康泰,等.高分子模板法合成特殊形态的氧化锌纳米结构材料[J].化学通报,2000(11):46-48
[26]Qian D.,Jiang J.Z.,Hansen P.L..Preparation of ZnO nanocrystals via ultrasonic irradiation[J].Chem.Commun.,2003(9):1078-1079
[27]沈国柱,徐政,朱英杰.不同形貌ZnO纳米粒子的超声化学法制备与表征[J].无机化学学报,2005,21(6):893-897
[28]王瑞华,李怀祥,张华,等.制备纳米发光氧化锌的新方法[J].纳米材料与结构,2004(2):23-25
[29]袁志好,孙永昌,别利剑,等.氧化锌纳米点阵列体系的制备及发光性能[J].无机化学学报,2004,20(9):1105-1108
[30]张贻瑞,王建.基础材料与新材料[M].天津:天津大学出版社,1994
[31]Rarig R.S.Jr.,Zubieta J..Hydrothermal synthesis and structural characterization of anorganic inorganic hybrid materials(H_2tptz)_2[δ_2Mo_8O_(26)]·2H_2O(tptz=2,4,6 tripyridyltriazine)[J].Inorganica Chimica Acta,2001,312:188-196
[32]Devi R.N.,Zubieta J..Synthesis and characterization of three novel inorganic/organic hybrid materials based on polyoxomolybdate duster:an investigation into the st ructural consequences of steric effect of the organoimine ligands[J].Inorganica Chimica Acta,2002,332:72-78
[33]Devi R.N.,Burkholder E.,Zubieta J..Hydrothermal synthesis of polyoxotung state clusters surface modified with M(Ⅱ)organonit rogen subunits[J].Inorganica Chimica Acta,2003,348:150-156
[34]Xu L.,Li M.,Wang E..Nanosized inorganic organic hybrid between polyoxometalate anion [PW_9Co_3O_(37)]~9 and pphenylenediamine[J].Mater Lett,2002,54:303-308
[35]Bourgeat-Lami E..Organic-inorganic nanostructured colloids[J].J.Nanosci Nanotechnol,2002,2(1):311-324
[36]倪克钒,单国荣,翁志学.Elaboration of hybrid organic-inorganic nanoparticles[J].Polymer Bulletin,2006(11):58-62
[37]孙丽宁,符连社,刘丰祎,等.Development of study on inorganic/organic hybrid luminescent materials doped with rare earth complex[J].发光学报,2005,26(1):15-26
[38]Quaroni L.,Chumanov G..Preparation of polymer-coated functionalized silver nanoparticles [J].J Am Chem Soc,1999,121:10642-10643
[39]Bourgeat-Lami E.,Espiard Ph.,Guyot A..Poly(ethyl acrylate)latexes encapsulating nanopartieles of silica:1.Functionalization and dispersion of silica[J].Polymer,1995,36(23):4385-4389
[40]Espiard Ph.,Guyot A.,Perez J.,etal..Poly(ethyl acrylate)latexes encapsulating nanoparticles of silica:3.Morphology and mechanical properties of reinforced films[J].Polymer,1995,36(23):4397-4403
[41]Bougeat-Lami E.,Lang J..Encapsulation of inorganic particles by dispersion polymerization in polar media:1.Silica nanopartieles encapsulated by polystyrene[J].J Colloid Interface Sei,1998,197:293-308
[42]Beaudry C.L.,Klein L.C..Sol-gel process of silica/poly(vinylacetate)nanocomposites[J].Polym Polym Comp,1995,3:431-432
[43]Wen J.Y.,Wilkes G.L.,Organic/inorganic hybrid net work materials by the sol-gel approach[J].Chem Mater,1996,8(8):1667-1681
[44]邵鑫,田军.有机-无机纳米复合材料的合成、性质及应用前景[J].材料导报,2001,15(1):50-53
[45]蒋葵阳,张隽,桂琳琳.PMMA-ZrO_2等有机无机杂化材料的制备与表征[J].物理化学学报,1997,13(5):407-412
[46]张隽,罗胜成,桂琳琳.PMMA-TiO_2有机无机杂化玻璃的制备与表征[J].物理化学学报,1996,13(4):289-292
[47]Jin Z.G.,Bu S.J.,Sun Y.C.,et al..Preparation and optical characteristics of films by chelating sol-gel method[J].Rare Metals,2004,23(3):214-219
[48]赵竹第,高宗明,欧玉春,等.苯乙烯-马来酸酐共聚物/聚硅氧烷纳米尺度复合材料的研究[J].高分子学报,1996,2:228-233
[49]应圣康,袁荞龙,喻志刚.中国专利申请号:99119829.8
[50]Eusworkth U.W.,Novak B.M..Mutually interpenetrating inorganic-organic networks,new routes into nonshrinking sol-gel composite materials[J].J Am Chem Soc,1991,113:2756-2758
[51]Novak B.M.,Grobbs R.H..Catalytic organometallie chemistry in water:The aqueous ringopening matathesis polymerization of 7-oxanorbomene derivatives[J].J Am Chem Soc,1988,110:7542-7543
[52]Muh S.W.,Pinnaviaia T..Synthesis and properties of organic-inorganic layered hybrid[J].J Chem Mater,1994,6:468-471
[53]Yano K.,Osuki A.,Okada A..Synthesis and properties ofpolyimide-clay hybrid film[J].J.Polym SciA:polym chem,1997,35(1):2289-2298
[54]赵竹第,李强,欧玉春,等.尼龙6/蒙脱土纳米复合材料的制备、结构与力学性能的研究[J].高分子学报,1997,5:519-522
[55]乔放,李强,漆宗能,等.聚酰胺/粘土纳米复合材料的制备、结构表征及性能研究[J].高分子通报,1997,3:135-137
[56]李强,赵竹第,欧玉春,等.尼龙6/蒙脱土纳米复合材料的结晶行为[J].高分子学报,1997,2:188-193
[57]Ruiz-Hitzky E..Conducting polymers intercalated in layered solids[J].Adv Mater,1993,5(5):334-340
[58]Wu J.,Lemer M.M..Structural,thermaland electrical characterization of layered nanocomposites derived from Na-uontm-orillonite and polyethers[J].Chem Mater,1993,5:835-838
[59]杨勇,朱子康,漆宗能.有机-无机纳米复合材料的研究进展[J].上海交通大学学报,1998,32(9):130-133
[60]Mousavand T.,Takami S.,Umetsu M.,et al..Supercritical hydrothermal synthesis of organicinorganic hybrid nanoparticles[J].J Mater Sci,2006,41(5):1445-1448
[61]Shang S.W.,Wiuiams J.W.,et al..Preparation and properties of EVA/SiO_2 hybrid material[J].J Mater Sci,1992,27:4949-4954
[62]张立群,王一中,王益庆.聚合物/无机物纳米复合胶乳的制备与性能研究[J].特种橡胶制品,1998,19(2):6-10
[63]邹小平,张良莹,姚熹,等.溶胶.凝胶法有机-无机精细复合材料P(VDF/TeFE)-SiO_2的制备与显微结构[J].功能材料,1998,29(3):327-329
[64]Suzuki F.,Onozato K..A formation of compatible poly(vinglacohol)/alumina gel composite and its properties[J].J Appl Polym Sci,1990,39:371-381
[65]No-Hyung Park,Kyung-Dusuh.Polyethylene toughened by CaCO_3 particle:Brittle-ductile transition of CaCO_3 toughened HDPE[J].J Appl Polym Sci,1996,71:1597-156l
[66]Vaia R.A.,Giamnelis E.P..Synthesis and properties of two-uimensional nanostruetues by direct intercalation of polymer melts in layered silicates[J].Chem Mater,1993,5:1694-1696
[67]胡平,范守善,万建伟.碳纳米管/UHMWPE复合材料的研究[J].工程塑料应用,1998,26(1):1-3
[68]Liu Y.,Yang Y.,Qian G.D.,et al..Energy transfer processes from Tb~(3+)to Eu~(3+)in ternary chelate doped in gel glasses via in situ technique[J].Materials Science and Engineering:B,2007,137(1-3):74-79
[69]Li H.R.,Lin J.,Zhang H.J.,et al..Preparation and luminescence properties of hybrid materials containing europium(Ⅲ)complexes eovalently bonded to a silica matrix[J].Chem.Meter.,2002,14:3651-3655
[70]Ashfold M.N.R..,Claeyssens F,Fuge G.M.,et al..Pulsed laser ablation and deposition of thin films[J].Chem.Soc.Rev.,2004,33:23-31
[71]詹勇军,吴卫东,王锋,等.NaF薄膜的脉冲激光沉积法制备与结构研究[J].强激光与粒子束,2007,19(4):633-637
[72]石明吉,李消山,孔祥贵.脉冲激光沉积法制备的纳米硅薄膜的结构与光学性质[J].发光学报,2006,27(6):981-986
[73]孙景,雷贻文,杜希文,等.用激光法合成纳米金刚石[J].材料研究学报,2006,20(1):33-36
[74]王伟田,关东仪,周岳亮,等.金属Fe薄膜的PLD制备及其非线性光学性质研究[J].物理学报,2005,54(7):3429-3433
[75]张兵临,覃东杰,徐彬,等.SnO_2薄膜的脉冲激光沉积[J].光电子·激光,1995,6(1):39-42
[76]苏凤莲,汪洪,李爱侠,等.用PLD法在MgO(100)衬底上生长ZnO薄膜的结构和光学特性[J].安徽大学学报(自然科学版),2006,30(2):67-70
[77]敖育红,胡少六,龙华,等.脉冲激光沉积薄膜技术研究新进展[J].激光技术,2003,27(5):453-459
[78]郭延龙,王小兵,万强,等.超快脉冲激光沉积类金刚石膜的研究进展[J].激光与光电子学进展,2005,42(7):22-25
[79]蒋娜娜,邵天敏,陈大融,等.利用脉冲激光真空弧沉积技术制备类金刚石薄膜[J].无机材料学报,2005,20(1):187-192.
[80]Willmott P.R.,Spillmann H.,Huber J.R.,et al..Design and systhesis of novel thin films and structures by reactive crossed-beam laser ablation[J].J.Mater.Chem.,2002,12:397-402
[81]Merel P.,Chaker M.,Tabbal M.,et al..Structural and electrical characteristics of epitaxial GaN thin films grown using pulsed laser deposition assisted by an atomic nitrogen source[J].Appl.Surf.Sci.,2001,177:165-171
[82]Sun X.W.,Xiao R.F.,Kwok H.S..Epitaxial growth of GaN thin film on sapphire with a thin ZnO buffer layer by liquid target pulsed laser deposition[J].J.Appl.Phys.,1998,84(10):5776-5779
[83]Cole D.,Lunney J.G..GaN thin films deposited by pulsed laser ablation in nitrogen and ammonia reactive atmospheres[J].Materials Science and Engineering,1997,B50:20-24
[84]Kawasaki K.,Despres J.F.,Kamei S.,et al..Fabrication of nanometer-sized anatase particles by a pulsed laser ablation method[J].J.Mater.Chem.,1997,7(10):2117-2120
[85]周异男,周勇,闫福林.脉冲激光溅射合成八-甲基硅倍半氧烷[J].化学工程师,2000,(4):28-29
[86]周异男,王改平,阎福林.激光溅射下聚甲基硅氧烷的结构重组[J].河南师范大学学报(自然科学版),2000,28(3):60-61
[87]汪洪海,郑启光,丘军林.反应淀积氮化铝薄膜及其性质的研究[J].中国激光,1999,26(1):89-92
[88]刘耀东,赵磊.脉冲激光沉积法制备氧化锌薄膜[J].中国激光,2007,34(4):534-537
[89]Ogale S.B.,Patil P.P.,Phase D.M.,et al..Synthesis of metastable phases via pulsed laser induced reactive quenching at liquid solid Interfaces[J].Phys Rev B,1987,36(16):8237-8250
[90]Ogale S.B.,Polman A.,Quentin F.O.P.,et al..Pulsed laser oxidization and nitridation of metal surface immersed in liquid media[J].Appl Phys Lett,1987,50(3):138-140
[91]Tokura H,Hidai H.Chemical machining by laser beam irradiation[J].International Journal of the Japan Society for Precision Engineering,1999,33(4):271-275
[92]齐飞,黄荣彬,郑兰荪,等.激光溅射产生团簇负离子[J].中国科学技术大学学报,1995,25(3):258-263
[93]张强,黄荣彬,郑兰荪,等.硫化钼纳米管的激光真空溅射产生[J].高等学校化学学报,1995,16(10):1624-1625
[94]王金斌,刘秋香,杨国伟,等.液体中激光烧蚀固体靶制备纳米晶金刚石[J].高压物理学报,1998,12(4):303-306
[95]王金斌,刘秋香,杨国伟,等.脉冲激光诱导液—固界面反应制备金刚石纳米晶[J].材料研究学报,1998,12(3):323-325
[96]钟向丽,王金斌,张灿云,等.液-固界面反应法制备c-BN纳米晶[J].功能材料,2004,2(35):186-187
[97]王金斌,杨国伟.脉冲激光诱导液-固界面反应合成金刚石纳米晶中的结构相变模型[J].高压物理学报,1999,13(2):147-151
[98]丁丽萍,方炎.Ag、Au纳米颗粒的激光表面修饰[J].光电子激光,2006,17(11):1377-1380
[99]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation and size control of silver nanoparticles by laser ablation in aqueous solution[J].J.Phys.Chem.B.,2000,104:9111-9117
[100]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Structure and stability of silver nanopartieles in aqueous solution produced by laser ablation[J].J.Phys.Chem.B.,2000,104:8333-8337
[101]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation of gold nanoparticles by laser ablation in aqueous solution of surfactant[J].J.Phys.Chem.B.,2001,105:5114-5120
[102]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Full physical preparation of size-selected gold nanoparticles in solution:laser ablation and laser-induced size control[J].J.Phys.Chem.B.,2002,106:7575-7577
[103]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Growth of gold clusters into nanoparticles in a solution following laser-induced fragmentation[J].J.Phys.Chem.B.,2002,106:8555-8561
[104]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Nanoscale soldering of metal nanopartieles for construction of high-order structures[J].J.Am.Chem.Sot.,2003,125:1686-1687
[105]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation of gold nanonetworks andsmall gold nanoparticles by irradiation of intense pulsed laser onto gold nanoparticles[J].J.Phys.Chem.B.,2003,107:12589-12596
[106]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation of stable platinum nanoparticles by laser ablation in water[J].J.Phys.Chem.B.,2003,107:4218-4223
[107]Peng Z.,Walther T.,Kleinermarms K..Influence of intense pulsed laser irradiation on optical and morphological properties of gold nanoparticle aggregates produced by surface acid-base reactions[J].Langrnuir,2005,21(10):4249-4253
[108]Compagnini G.,Scalisi A.A.,Puglisi O..Nonlinear optical activity in Ag-SiO_2 nanocomposite thin films with different silver concentration[J].Phys.Chem.Chem.Phys.,2002,(4):2787-2791
[109]Iwabuchi A.,Choo C.K.,Tanaka K..Titania nanoparticles prepared with pulsed laser ablation of rutile single crystals in water[J].J.Phys.Chem.,2004,108:10863-10871
[110]Liang C.H.,Shimizu Y.,Masuda M.,et al..Synthesis of ultrafine SnO_(2-x)nanocrystals by pulsed laser-induced reactive quenching in liquid medium[J].J.Phys.Chem.,2003,107:9220-9225
[111]Liang C.H.,Shimizu Y.,Masuda M.,et al..Preparation of layered zinc hydroxide/surfaetant nanocomposite by pulsed-laser ablation in a liquid medium[J].Chem.Mater.,2004,16(6):963-965
[112]Lee Y.P.,Liu Y.H.,Yeh C.S..Formation of bayerite,gibbsite and boehmite particles by laser ablation[J].Phys.Chem.Chem.Phys.,1999,1:4681-4686
[113]余乐,姚佳,傅正文.液相脉冲激光烧蚀法制备高熔点的纳米金属粒子[J].物理化学学报,2007,23(6):945-949
[114]雷贻文,孙景,杜希文,等.低功率密度激光合成金刚石的相变机制[J].中国激光,2007,34(2):295-299
[115]王金斌,刘秋香,杨国伟.脉冲激光诱导液-固界面反应制备立方相C_3N_4纳米晶[J].高等学校化学学报,1998,19(11):1719-1720
[116]任志昂,王金斌,刘秋香,等.脉冲激光诱导液-固界面反应制备石墨相C_3N_4[J].光电子·激光,2001(2):164-166
[117]Zhang W.G.,Zhang Y.,Tang J.,et al..Study on the preparation of novel nano-rare earth oxides/organic polymer hybrid films and their optical properties,In:International Conference on Materials for Advanced Technologies,Singapore[C],2001,232
[118]Zhang W.G.,zhang Y.,Tang J.,et al..Study on preparation and optic properties of nano europium oxide-ethanol sol by pulsed Laser ablation[J].Thin Solid Films,2002,417:43-46
[119]章仪,陈文哲,章文贡.脉冲激光法连续制备纳米钴乙醇溶胶的研究[J].高等学校化学学报,2003,24(2):337-339
[120]章仪,陈文哲,章文贡.脉冲激光法连续制备纳米铁溶胶及其分散稳性的研究[J].化学学报,2003,61(1):141-145
[121]陈莲英,章文贡.脉冲激光轰击法连续制备纳米铜研究[J].化工科技,2004,12(2):1-5
[122]章文贡,金兆国.激光法连续制备纳米FeNi合金及其乙醇溶胶的研究[J].中国科学(B辑),2003,33(6):527-533
[123]林爱梅,陈长鑫,陈文哲.脉冲激光轰击制备碳纳米管及其纳米溶胶的研究[J].机电技术,2003.S1:297-301
[124]Chen C.X.,Chen W.Z.,Zhang Y.F..Synthesis of carbon nano-tubcs by pulsed laser ablation at normal pressure in metal nano-sol[J].Physica E.,2005,28(2):121-127
[125]Chen Q.H.,Zhang W.G.,Huang X.X..Study on continuous preparation of nano europium oxide ethanol sols decorated in situ by pulsed laser ablation and their luminescence characteristics[J].Optical Materials,2007,Accepted.
[126]Chcn Q.H.,Zhang W.G.,Huang X.X..Study on the surface decorating of nano Tb_2O_3 in the ethanol sol and its fluorescence characteristics[J].Journal of Luminescence(2006),doi:10.1016/j.jlumin.200607010.
[127]Chcn Q.H.,Zhang W.G..Successive preparation of decorated zinc oxide organic sol by pulsed laser ablation and their luminescence characteristics[J].Apply Surface Science.2006,253:3751-3756
[128]Chen Q.H.,Zhang W.G..Study on preparation and fluorescence characteristic of the (Alqx)/Al2O3 nano colloids[J].J.Colloid and Interface Science(2006),doi:10.1016/j.jcis.2006.10.069
[129]金兆国,章文贡.脉冲激光轰击法原位制备纳米碳/聚苯乙烯杂化材料的研究[J].中国塑料,2004,18(6):48-53
[130]程文德,吴萍.具有四角锥状纳米ZnO的制备及强蓝光发射特性[J].发光学报,2006,27(4):608-613
[131]郭书霞,张兴堂,赵慧玲,等.纳米氧化锌的制备与发光性能的研究[J].无机化学学报,2006,21(4):754-728
[132]Abdullah M.,Morimoto T.,Okuyama k..Generating blue and red luminescence from ZnO/Poly(ethyleneglycol)nanocomposites prepared using an on-situ method[J].Adv.Funct.Mater.,2003,13(10):800-804
[133]Wang Y.D.,Zhang S.,Wu X.H..Green light luminescence from ZnO/Dodecylamine mesolamellar nanocornposites synthesized by self-assembly[J].Eur.J.Inorg.Chem.,2005(4):727-731
[134]陈宝玲,赵立新,张冰,等.大功率激光制备a-C和a-C:H类金刚石膜的光学性能研究[J].高等学校化学学报,2006,27(6):1012-1025
[135]贾少杰,徐抒平,郑先亮,等.激光诱导沉积银膜制备光纤SERS传感器[J].高等学校化学学报,2006,27(3):523-526
[136]Sun J.,Xie W.,Yuan L.G.,et al..Preparation and luminescence properties of Tb~(3+)doped zinc salicylates Materials[J].Science and Engineering,1999,B64:157-160
[137]Wlodzimierz L.,Halina B..The influence of selected metals on the arom tic system of salicylic acid[J].Applied Spectroscopy,1987,41(6):976-979
[138]Hegetschweiler K.,Finn R.C.,Zubieta J..Surface complexation of[Nb6_O_(19)]8~- with Ni~(Ⅱ):solvethermal syntheis and X-ray structural characterization of the two novel heterometallic Ni_2Nb_2polyoxometalates[J].InorganicaChimica Acta,2002,337:39-47
[139]Rarig R.S.Jr.,Bewley L.,Zubieta J..Hydrothermal synthesis and characterization of a novel bimetallic polyoxocation,[Cu_6(dtbbpy)_6Mo_7O_(26)]~(2+)(dtbbpy=4,4'ditcrt-butyl-2,2'- bipyridine)[J].Inorganic Chemistry Communications,2003(6):539-542
[140]Carlucci L.,Ciani G.,Proserpio D.M..New polymeric networks from the self-assembly of silver(Ⅰ)salts and the flexible ligand 1,3-bis(4-pyridyl)propane(bpp):A systematic investigation of the effects of the counterions and a survey of the coordination polymers based on bpp[J].Cryst Eng Comm,2002,4:121-129
[141]Gehr R.J.,Boyd R.W..Optical properties of nano structured materials[J].Chem Mater,1996,8(8):1807-1819
[142]Vestal C.R.,Zhang Z,J..Atom transfer radical polymerization synthesis and magnetic characterization of MnFe_2O_4/polystyrene core/shell nanoparticles[J].J Am Chem Soc,2002,124(48):14312-14313
[143]Chert X.,Randall D.P.,Perruchot C.,et al..Synthesis and aqueous solution properties of polyelect rolyte-grafted silica particles prepared by surface-initiated atom t ransfer radical polymerization[J].J.Colloid Interf Sci,2003,257(1):56-59
[144]Mousavand T.,Takami S.,Umetsu M.,et al..Supercritical hydrothermal synthesis of organicinorganic hybrid nanoparticles[J].J Mater Sci,2006,41(5):1445-1447
[145]Orialchi C.O.,Lemer M.M..Poly(pyrrole)and poly(thiophene)/clay nanoeomposites[J].Mater Res Bull,1995,30(6):723-729
[146]肖旺钏,章文贡.脉冲激光轰击法连续制备C_(60)原位修饰铜团簇杂化材料的研究[J].无机化学学报,2006,22(4):666-672
[147]Burroughes J.H.,Bradley D.D.C.,Brown A.R.,et al..Light-emitting diodes based on conjugated polymers[J].Nature,1990,347(6293):539-541
[148]Kido J.,Shionoya H.,Nagai K..Single-layer white light-emitting organic eleetrolumineseent devices based on dye-dispersed poly(N-vinylcarbazole)[J].Appl.Phys.Lett.,1995,67(16):2281-2283
[149]Berggren M.,Inganas O.,Gustafsson G.,et al..Light-emitting-diodes with variable Colors from polymer blends[J].Nature,1994,372(6505):444-446
[150]Tu G.L.,Zhou Q.G.,Cheng Y.X.,et al..White electroluminescence from polyfluorene chemically doped with 1,8-napthalimide moieties[J].Appl.Phys.Lett.,2004,85(12):2172-2174.
[151]Xu Q.F.,Duong H.M.,Fred W.,et al..Efficient single-layer "twistacene"-doped polymer white light-emitting diodes[J].Appl.Phys.Lett.,2004,85(16):3357-3359
[152]朱明华编.仪器分析(第三版)[M].高等教育出版社,2000:275
[2]Zu P.,Tang Z.K.,Kawasaki M.,et al..Ultraviolet spontaneous and stimulated emission from ZnO micro crystalline thin films at room temperature[J].Solid State Com,1997,103(8):459-463
[3]Du Y.,Zang M.S.,Hong J.,et al..Structural and optical properties of nanophase zinc oxide[J].Applied Physics A.2003,76:171-176
[4]Dierstein A.,Natter H.,Meyer F.,et al..Electrochemical deposition under oxidizing conditions (EDOC):a new synthesis for nanocrystalline metal oxides[J].Scripta mater,2001,44(8/9):2209-2212
[5]Posner E.G..Colloidal zinc oxide[P].US24359,1995,9(14)
[6]朱勇,沈辉,刘佩田,等.激光加热制备ZnO纳米粉[J].无机材料学报,1993,8(1):111-113
[7]Thangaraju B..Structural and electrical studies on highly conducting spray deposited fluorine and antimony doped SnO_2 thin films from SnCl_2 precursor[J].Thin Solid Films,2002,402(1-2):71-78
[8]赵新宇,郑柏存,李春中,等.喷雾热解合成ZnO超细粒子工艺及机理研究[J].无机材料学报,1996,11(4):611-616
[9]俞建群,贾殿赠,郑毓锋,等.纳米氧化镍,氧化锌的合成新方法[J].无机化学学报,1999,15(1):95-98
[10]沈茹娟,贾殿赠,梁凯,等.纳米氧化锌的固相合成及其气敏特性[J].无机化学学报,2000,16(6):906-910
[11]Takuya T.,Paul G M..ZnO nanoparticles synthesised by mechanochemical processing[J].Scripta mater,2001,44(8/9):1731-1734
[12]黄志明,刘建斌,许民.纳米氧化锌的固相合成[J].有色金属,2004(1):41-43
[13]亓秀芹,陶栋梁,黄毅,等.氧化锌纳米棒的生长过程研究[J].光谱学与光谱分析,2005,25(3):321-325
[14]张士成,李春和,李星.纳米氧化锌的粒度控制与表征[J].物理化学学报,2004,20(8):902-905
[15]罗志强,张孝彬,程继鹏,等.化学溶液沉积法制备单分散氧化锌纳米棒阵列[J].化学学报,2005,63(18):1656-1660
[16]杨青林,郭林,吴中华,等.室温下纳米氧化锌新相的合成及表征[J].高等化学学报,2003(24):82-85
[17]徐甲强,潘庆谊,孙雨安,等.纳米氧化锌的乳液合成,结构表征与气敏性能[J].无机化学学报,1998,14(3):355-359
[18]Yu B.L.,Zou B.S.,Wu X.C..Preparation of ZnO nanometer powder and their ESR properties [J].Chinese Journal of Semiconductors,1995,16(7):558-560
[19]Daisuke K.,Hideki S.,Takeshi K.,et al..Synthesis of ZnO particles by ammonia-catalyzed hydrolysis of Zinc dibutoxide in nonionic reversed micelles[J].Langmuir,2000,16(9):4086-4089
[20]陈友存,张元广,周根.棒状和球状氧化锌微晶的控制合成及其表征[J].无机材料学报,2004,19(5):1173-1176
[21]李汶军,施尔畏,王步国,等.水热法制备氧化锌粉体[J].无机材料学报,1998,13(1):27-32
[22]徐甲强,纪朋,李志伟,等.水热法合成氧化锌亚微米棒及气敏性能研究[J].郑州轻工业学院学报(自然科学版),2005,20(3):1-3
[23]郭敏,刁鹏,蔡生民.水热法制备高度取向的氧化锌纳米棒阵列[J].高等学校化学学报,2004,2(2):345-347
[24]宋旭春,徐铸德,陈卫祥,等.氧化锌纳米棒的制备和生长机理研究[J].无机化学学报,2004,20(2):186-190
[25]刘雪宁,杨治中,唐康泰,等.高分子模板法合成特殊形态的氧化锌纳米结构材料[J].化学通报,2000(11):46-48
[26]Qian D.,Jiang J.Z.,Hansen P.L..Preparation of ZnO nanocrystals via ultrasonic irradiation[J].Chem.Commun.,2003(9):1078-1079
[27]沈国柱,徐政,朱英杰.不同形貌ZnO纳米粒子的超声化学法制备与表征[J].无机化学学报,2005,21(6):893-897
[28]王瑞华,李怀祥,张华,等.制备纳米发光氧化锌的新方法[J].纳米材料与结构,2004(2):23-25
[29]袁志好,孙永昌,别利剑,等.氧化锌纳米点阵列体系的制备及发光性能[J].无机化学学报,2004,20(9):1105-1108
[30]张贻瑞,王建.基础材料与新材料[M].天津:天津大学出版社,1994
[31]Rarig R.S.Jr.,Zubieta J..Hydrothermal synthesis and structural characterization of anorganic inorganic hybrid materials(H_2tptz)_2[δ_2Mo_8O_(26)]·2H_2O(tptz=2,4,6 tripyridyltriazine)[J].Inorganica Chimica Acta,2001,312:188-196
[32]Devi R.N.,Zubieta J..Synthesis and characterization of three novel inorganic/organic hybrid materials based on polyoxomolybdate duster:an investigation into the st ructural consequences of steric effect of the organoimine ligands[J].Inorganica Chimica Acta,2002,332:72-78
[33]Devi R.N.,Burkholder E.,Zubieta J..Hydrothermal synthesis of polyoxotung state clusters surface modified with M(Ⅱ)organonit rogen subunits[J].Inorganica Chimica Acta,2003,348:150-156
[34]Xu L.,Li M.,Wang E..Nanosized inorganic organic hybrid between polyoxometalate anion [PW_9Co_3O_(37)]~9 and pphenylenediamine[J].Mater Lett,2002,54:303-308
[35]Bourgeat-Lami E..Organic-inorganic nanostructured colloids[J].J.Nanosci Nanotechnol,2002,2(1):311-324
[36]倪克钒,单国荣,翁志学.Elaboration of hybrid organic-inorganic nanoparticles[J].Polymer Bulletin,2006(11):58-62
[37]孙丽宁,符连社,刘丰祎,等.Development of study on inorganic/organic hybrid luminescent materials doped with rare earth complex[J].发光学报,2005,26(1):15-26
[38]Quaroni L.,Chumanov G..Preparation of polymer-coated functionalized silver nanoparticles [J].J Am Chem Soc,1999,121:10642-10643
[39]Bourgeat-Lami E.,Espiard Ph.,Guyot A..Poly(ethyl acrylate)latexes encapsulating nanopartieles of silica:1.Functionalization and dispersion of silica[J].Polymer,1995,36(23):4385-4389
[40]Espiard Ph.,Guyot A.,Perez J.,etal..Poly(ethyl acrylate)latexes encapsulating nanoparticles of silica:3.Morphology and mechanical properties of reinforced films[J].Polymer,1995,36(23):4397-4403
[41]Bougeat-Lami E.,Lang J..Encapsulation of inorganic particles by dispersion polymerization in polar media:1.Silica nanopartieles encapsulated by polystyrene[J].J Colloid Interface Sei,1998,197:293-308
[42]Beaudry C.L.,Klein L.C..Sol-gel process of silica/poly(vinylacetate)nanocomposites[J].Polym Polym Comp,1995,3:431-432
[43]Wen J.Y.,Wilkes G.L.,Organic/inorganic hybrid net work materials by the sol-gel approach[J].Chem Mater,1996,8(8):1667-1681
[44]邵鑫,田军.有机-无机纳米复合材料的合成、性质及应用前景[J].材料导报,2001,15(1):50-53
[45]蒋葵阳,张隽,桂琳琳.PMMA-ZrO_2等有机无机杂化材料的制备与表征[J].物理化学学报,1997,13(5):407-412
[46]张隽,罗胜成,桂琳琳.PMMA-TiO_2有机无机杂化玻璃的制备与表征[J].物理化学学报,1996,13(4):289-292
[47]Jin Z.G.,Bu S.J.,Sun Y.C.,et al..Preparation and optical characteristics of films by chelating sol-gel method[J].Rare Metals,2004,23(3):214-219
[48]赵竹第,高宗明,欧玉春,等.苯乙烯-马来酸酐共聚物/聚硅氧烷纳米尺度复合材料的研究[J].高分子学报,1996,2:228-233
[49]应圣康,袁荞龙,喻志刚.中国专利申请号:99119829.8
[50]Eusworkth U.W.,Novak B.M..Mutually interpenetrating inorganic-organic networks,new routes into nonshrinking sol-gel composite materials[J].J Am Chem Soc,1991,113:2756-2758
[51]Novak B.M.,Grobbs R.H..Catalytic organometallie chemistry in water:The aqueous ringopening matathesis polymerization of 7-oxanorbomene derivatives[J].J Am Chem Soc,1988,110:7542-7543
[52]Muh S.W.,Pinnaviaia T..Synthesis and properties of organic-inorganic layered hybrid[J].J Chem Mater,1994,6:468-471
[53]Yano K.,Osuki A.,Okada A..Synthesis and properties ofpolyimide-clay hybrid film[J].J.Polym SciA:polym chem,1997,35(1):2289-2298
[54]赵竹第,李强,欧玉春,等.尼龙6/蒙脱土纳米复合材料的制备、结构与力学性能的研究[J].高分子学报,1997,5:519-522
[55]乔放,李强,漆宗能,等.聚酰胺/粘土纳米复合材料的制备、结构表征及性能研究[J].高分子通报,1997,3:135-137
[56]李强,赵竹第,欧玉春,等.尼龙6/蒙脱土纳米复合材料的结晶行为[J].高分子学报,1997,2:188-193
[57]Ruiz-Hitzky E..Conducting polymers intercalated in layered solids[J].Adv Mater,1993,5(5):334-340
[58]Wu J.,Lemer M.M..Structural,thermaland electrical characterization of layered nanocomposites derived from Na-uontm-orillonite and polyethers[J].Chem Mater,1993,5:835-838
[59]杨勇,朱子康,漆宗能.有机-无机纳米复合材料的研究进展[J].上海交通大学学报,1998,32(9):130-133
[60]Mousavand T.,Takami S.,Umetsu M.,et al..Supercritical hydrothermal synthesis of organicinorganic hybrid nanoparticles[J].J Mater Sci,2006,41(5):1445-1448
[61]Shang S.W.,Wiuiams J.W.,et al..Preparation and properties of EVA/SiO_2 hybrid material[J].J Mater Sci,1992,27:4949-4954
[62]张立群,王一中,王益庆.聚合物/无机物纳米复合胶乳的制备与性能研究[J].特种橡胶制品,1998,19(2):6-10
[63]邹小平,张良莹,姚熹,等.溶胶.凝胶法有机-无机精细复合材料P(VDF/TeFE)-SiO_2的制备与显微结构[J].功能材料,1998,29(3):327-329
[64]Suzuki F.,Onozato K..A formation of compatible poly(vinglacohol)/alumina gel composite and its properties[J].J Appl Polym Sci,1990,39:371-381
[65]No-Hyung Park,Kyung-Dusuh.Polyethylene toughened by CaCO_3 particle:Brittle-ductile transition of CaCO_3 toughened HDPE[J].J Appl Polym Sci,1996,71:1597-156l
[66]Vaia R.A.,Giamnelis E.P..Synthesis and properties of two-uimensional nanostruetues by direct intercalation of polymer melts in layered silicates[J].Chem Mater,1993,5:1694-1696
[67]胡平,范守善,万建伟.碳纳米管/UHMWPE复合材料的研究[J].工程塑料应用,1998,26(1):1-3
[68]Liu Y.,Yang Y.,Qian G.D.,et al..Energy transfer processes from Tb~(3+)to Eu~(3+)in ternary chelate doped in gel glasses via in situ technique[J].Materials Science and Engineering:B,2007,137(1-3):74-79
[69]Li H.R.,Lin J.,Zhang H.J.,et al..Preparation and luminescence properties of hybrid materials containing europium(Ⅲ)complexes eovalently bonded to a silica matrix[J].Chem.Meter.,2002,14:3651-3655
[70]Ashfold M.N.R..,Claeyssens F,Fuge G.M.,et al..Pulsed laser ablation and deposition of thin films[J].Chem.Soc.Rev.,2004,33:23-31
[71]詹勇军,吴卫东,王锋,等.NaF薄膜的脉冲激光沉积法制备与结构研究[J].强激光与粒子束,2007,19(4):633-637
[72]石明吉,李消山,孔祥贵.脉冲激光沉积法制备的纳米硅薄膜的结构与光学性质[J].发光学报,2006,27(6):981-986
[73]孙景,雷贻文,杜希文,等.用激光法合成纳米金刚石[J].材料研究学报,2006,20(1):33-36
[74]王伟田,关东仪,周岳亮,等.金属Fe薄膜的PLD制备及其非线性光学性质研究[J].物理学报,2005,54(7):3429-3433
[75]张兵临,覃东杰,徐彬,等.SnO_2薄膜的脉冲激光沉积[J].光电子·激光,1995,6(1):39-42
[76]苏凤莲,汪洪,李爱侠,等.用PLD法在MgO(100)衬底上生长ZnO薄膜的结构和光学特性[J].安徽大学学报(自然科学版),2006,30(2):67-70
[77]敖育红,胡少六,龙华,等.脉冲激光沉积薄膜技术研究新进展[J].激光技术,2003,27(5):453-459
[78]郭延龙,王小兵,万强,等.超快脉冲激光沉积类金刚石膜的研究进展[J].激光与光电子学进展,2005,42(7):22-25
[79]蒋娜娜,邵天敏,陈大融,等.利用脉冲激光真空弧沉积技术制备类金刚石薄膜[J].无机材料学报,2005,20(1):187-192.
[80]Willmott P.R.,Spillmann H.,Huber J.R.,et al..Design and systhesis of novel thin films and structures by reactive crossed-beam laser ablation[J].J.Mater.Chem.,2002,12:397-402
[81]Merel P.,Chaker M.,Tabbal M.,et al..Structural and electrical characteristics of epitaxial GaN thin films grown using pulsed laser deposition assisted by an atomic nitrogen source[J].Appl.Surf.Sci.,2001,177:165-171
[82]Sun X.W.,Xiao R.F.,Kwok H.S..Epitaxial growth of GaN thin film on sapphire with a thin ZnO buffer layer by liquid target pulsed laser deposition[J].J.Appl.Phys.,1998,84(10):5776-5779
[83]Cole D.,Lunney J.G..GaN thin films deposited by pulsed laser ablation in nitrogen and ammonia reactive atmospheres[J].Materials Science and Engineering,1997,B50:20-24
[84]Kawasaki K.,Despres J.F.,Kamei S.,et al..Fabrication of nanometer-sized anatase particles by a pulsed laser ablation method[J].J.Mater.Chem.,1997,7(10):2117-2120
[85]周异男,周勇,闫福林.脉冲激光溅射合成八-甲基硅倍半氧烷[J].化学工程师,2000,(4):28-29
[86]周异男,王改平,阎福林.激光溅射下聚甲基硅氧烷的结构重组[J].河南师范大学学报(自然科学版),2000,28(3):60-61
[87]汪洪海,郑启光,丘军林.反应淀积氮化铝薄膜及其性质的研究[J].中国激光,1999,26(1):89-92
[88]刘耀东,赵磊.脉冲激光沉积法制备氧化锌薄膜[J].中国激光,2007,34(4):534-537
[89]Ogale S.B.,Patil P.P.,Phase D.M.,et al..Synthesis of metastable phases via pulsed laser induced reactive quenching at liquid solid Interfaces[J].Phys Rev B,1987,36(16):8237-8250
[90]Ogale S.B.,Polman A.,Quentin F.O.P.,et al..Pulsed laser oxidization and nitridation of metal surface immersed in liquid media[J].Appl Phys Lett,1987,50(3):138-140
[91]Tokura H,Hidai H.Chemical machining by laser beam irradiation[J].International Journal of the Japan Society for Precision Engineering,1999,33(4):271-275
[92]齐飞,黄荣彬,郑兰荪,等.激光溅射产生团簇负离子[J].中国科学技术大学学报,1995,25(3):258-263
[93]张强,黄荣彬,郑兰荪,等.硫化钼纳米管的激光真空溅射产生[J].高等学校化学学报,1995,16(10):1624-1625
[94]王金斌,刘秋香,杨国伟,等.液体中激光烧蚀固体靶制备纳米晶金刚石[J].高压物理学报,1998,12(4):303-306
[95]王金斌,刘秋香,杨国伟,等.脉冲激光诱导液—固界面反应制备金刚石纳米晶[J].材料研究学报,1998,12(3):323-325
[96]钟向丽,王金斌,张灿云,等.液-固界面反应法制备c-BN纳米晶[J].功能材料,2004,2(35):186-187
[97]王金斌,杨国伟.脉冲激光诱导液-固界面反应合成金刚石纳米晶中的结构相变模型[J].高压物理学报,1999,13(2):147-151
[98]丁丽萍,方炎.Ag、Au纳米颗粒的激光表面修饰[J].光电子激光,2006,17(11):1377-1380
[99]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation and size control of silver nanoparticles by laser ablation in aqueous solution[J].J.Phys.Chem.B.,2000,104:9111-9117
[100]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Structure and stability of silver nanopartieles in aqueous solution produced by laser ablation[J].J.Phys.Chem.B.,2000,104:8333-8337
[101]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation of gold nanoparticles by laser ablation in aqueous solution of surfactant[J].J.Phys.Chem.B.,2001,105:5114-5120
[102]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Full physical preparation of size-selected gold nanoparticles in solution:laser ablation and laser-induced size control[J].J.Phys.Chem.B.,2002,106:7575-7577
[103]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Growth of gold clusters into nanoparticles in a solution following laser-induced fragmentation[J].J.Phys.Chem.B.,2002,106:8555-8561
[104]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Nanoscale soldering of metal nanopartieles for construction of high-order structures[J].J.Am.Chem.Sot.,2003,125:1686-1687
[105]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation of gold nanonetworks andsmall gold nanoparticles by irradiation of intense pulsed laser onto gold nanoparticles[J].J.Phys.Chem.B.,2003,107:12589-12596
[106]Mafune F.,Kohno J.Y.,Takeda Y.,et al..Formation of stable platinum nanoparticles by laser ablation in water[J].J.Phys.Chem.B.,2003,107:4218-4223
[107]Peng Z.,Walther T.,Kleinermarms K..Influence of intense pulsed laser irradiation on optical and morphological properties of gold nanoparticle aggregates produced by surface acid-base reactions[J].Langrnuir,2005,21(10):4249-4253
[108]Compagnini G.,Scalisi A.A.,Puglisi O..Nonlinear optical activity in Ag-SiO_2 nanocomposite thin films with different silver concentration[J].Phys.Chem.Chem.Phys.,2002,(4):2787-2791
[109]Iwabuchi A.,Choo C.K.,Tanaka K..Titania nanoparticles prepared with pulsed laser ablation of rutile single crystals in water[J].J.Phys.Chem.,2004,108:10863-10871
[110]Liang C.H.,Shimizu Y.,Masuda M.,et al..Synthesis of ultrafine SnO_(2-x)nanocrystals by pulsed laser-induced reactive quenching in liquid medium[J].J.Phys.Chem.,2003,107:9220-9225
[111]Liang C.H.,Shimizu Y.,Masuda M.,et al..Preparation of layered zinc hydroxide/surfaetant nanocomposite by pulsed-laser ablation in a liquid medium[J].Chem.Mater.,2004,16(6):963-965
[112]Lee Y.P.,Liu Y.H.,Yeh C.S..Formation of bayerite,gibbsite and boehmite particles by laser ablation[J].Phys.Chem.Chem.Phys.,1999,1:4681-4686
[113]余乐,姚佳,傅正文.液相脉冲激光烧蚀法制备高熔点的纳米金属粒子[J].物理化学学报,2007,23(6):945-949
[114]雷贻文,孙景,杜希文,等.低功率密度激光合成金刚石的相变机制[J].中国激光,2007,34(2):295-299
[115]王金斌,刘秋香,杨国伟.脉冲激光诱导液-固界面反应制备立方相C_3N_4纳米晶[J].高等学校化学学报,1998,19(11):1719-1720
[116]任志昂,王金斌,刘秋香,等.脉冲激光诱导液-固界面反应制备石墨相C_3N_4[J].光电子·激光,2001(2):164-166
[117]Zhang W.G.,Zhang Y.,Tang J.,et al..Study on the preparation of novel nano-rare earth oxides/organic polymer hybrid films and their optical properties,In:International Conference on Materials for Advanced Technologies,Singapore[C],2001,232
[118]Zhang W.G.,zhang Y.,Tang J.,et al..Study on preparation and optic properties of nano europium oxide-ethanol sol by pulsed Laser ablation[J].Thin Solid Films,2002,417:43-46
[119]章仪,陈文哲,章文贡.脉冲激光法连续制备纳米钴乙醇溶胶的研究[J].高等学校化学学报,2003,24(2):337-339
[120]章仪,陈文哲,章文贡.脉冲激光法连续制备纳米铁溶胶及其分散稳性的研究[J].化学学报,2003,61(1):141-145
[121]陈莲英,章文贡.脉冲激光轰击法连续制备纳米铜研究[J].化工科技,2004,12(2):1-5
[122]章文贡,金兆国.激光法连续制备纳米FeNi合金及其乙醇溶胶的研究[J].中国科学(B辑),2003,33(6):527-533
[123]林爱梅,陈长鑫,陈文哲.脉冲激光轰击制备碳纳米管及其纳米溶胶的研究[J].机电技术,2003.S1:297-301
[124]Chen C.X.,Chen W.Z.,Zhang Y.F..Synthesis of carbon nano-tubcs by pulsed laser ablation at normal pressure in metal nano-sol[J].Physica E.,2005,28(2):121-127
[125]Chen Q.H.,Zhang W.G.,Huang X.X..Study on continuous preparation of nano europium oxide ethanol sols decorated in situ by pulsed laser ablation and their luminescence characteristics[J].Optical Materials,2007,Accepted.
[126]Chcn Q.H.,Zhang W.G.,Huang X.X..Study on the surface decorating of nano Tb_2O_3 in the ethanol sol and its fluorescence characteristics[J].Journal of Luminescence(2006),doi:10.1016/j.jlumin.200607010.
[127]Chcn Q.H.,Zhang W.G..Successive preparation of decorated zinc oxide organic sol by pulsed laser ablation and their luminescence characteristics[J].Apply Surface Science.2006,253:3751-3756
[128]Chen Q.H.,Zhang W.G..Study on preparation and fluorescence characteristic of the (Alqx)/Al2O3 nano colloids[J].J.Colloid and Interface Science(2006),doi:10.1016/j.jcis.2006.10.069
[129]金兆国,章文贡.脉冲激光轰击法原位制备纳米碳/聚苯乙烯杂化材料的研究[J].中国塑料,2004,18(6):48-53
[130]程文德,吴萍.具有四角锥状纳米ZnO的制备及强蓝光发射特性[J].发光学报,2006,27(4):608-613
[131]郭书霞,张兴堂,赵慧玲,等.纳米氧化锌的制备与发光性能的研究[J].无机化学学报,2006,21(4):754-728
[132]Abdullah M.,Morimoto T.,Okuyama k..Generating blue and red luminescence from ZnO/Poly(ethyleneglycol)nanocomposites prepared using an on-situ method[J].Adv.Funct.Mater.,2003,13(10):800-804
[133]Wang Y.D.,Zhang S.,Wu X.H..Green light luminescence from ZnO/Dodecylamine mesolamellar nanocornposites synthesized by self-assembly[J].Eur.J.Inorg.Chem.,2005(4):727-731
[134]陈宝玲,赵立新,张冰,等.大功率激光制备a-C和a-C:H类金刚石膜的光学性能研究[J].高等学校化学学报,2006,27(6):1012-1025
[135]贾少杰,徐抒平,郑先亮,等.激光诱导沉积银膜制备光纤SERS传感器[J].高等学校化学学报,2006,27(3):523-526
[136]Sun J.,Xie W.,Yuan L.G.,et al..Preparation and luminescence properties of Tb~(3+)doped zinc salicylates Materials[J].Science and Engineering,1999,B64:157-160
[137]Wlodzimierz L.,Halina B..The influence of selected metals on the arom tic system of salicylic acid[J].Applied Spectroscopy,1987,41(6):976-979
[138]Hegetschweiler K.,Finn R.C.,Zubieta J..Surface complexation of[Nb6_O_(19)]8~- with Ni~(Ⅱ):solvethermal syntheis and X-ray structural characterization of the two novel heterometallic Ni_2Nb_2polyoxometalates[J].InorganicaChimica Acta,2002,337:39-47
[139]Rarig R.S.Jr.,Bewley L.,Zubieta J..Hydrothermal synthesis and characterization of a novel bimetallic polyoxocation,[Cu_6(dtbbpy)_6Mo_7O_(26)]~(2+)(dtbbpy=4,4'ditcrt-butyl-2,2'- bipyridine)[J].Inorganic Chemistry Communications,2003(6):539-542
[140]Carlucci L.,Ciani G.,Proserpio D.M..New polymeric networks from the self-assembly of silver(Ⅰ)salts and the flexible ligand 1,3-bis(4-pyridyl)propane(bpp):A systematic investigation of the effects of the counterions and a survey of the coordination polymers based on bpp[J].Cryst Eng Comm,2002,4:121-129
[141]Gehr R.J.,Boyd R.W..Optical properties of nano structured materials[J].Chem Mater,1996,8(8):1807-1819
[142]Vestal C.R.,Zhang Z,J..Atom transfer radical polymerization synthesis and magnetic characterization of MnFe_2O_4/polystyrene core/shell nanoparticles[J].J Am Chem Soc,2002,124(48):14312-14313
[143]Chert X.,Randall D.P.,Perruchot C.,et al..Synthesis and aqueous solution properties of polyelect rolyte-grafted silica particles prepared by surface-initiated atom t ransfer radical polymerization[J].J.Colloid Interf Sci,2003,257(1):56-59
[144]Mousavand T.,Takami S.,Umetsu M.,et al..Supercritical hydrothermal synthesis of organicinorganic hybrid nanoparticles[J].J Mater Sci,2006,41(5):1445-1447
[145]Orialchi C.O.,Lemer M.M..Poly(pyrrole)and poly(thiophene)/clay nanoeomposites[J].Mater Res Bull,1995,30(6):723-729
[146]肖旺钏,章文贡.脉冲激光轰击法连续制备C_(60)原位修饰铜团簇杂化材料的研究[J].无机化学学报,2006,22(4):666-672
[147]Burroughes J.H.,Bradley D.D.C.,Brown A.R.,et al..Light-emitting diodes based on conjugated polymers[J].Nature,1990,347(6293):539-541
[148]Kido J.,Shionoya H.,Nagai K..Single-layer white light-emitting organic eleetrolumineseent devices based on dye-dispersed poly(N-vinylcarbazole)[J].Appl.Phys.Lett.,1995,67(16):2281-2283
[149]Berggren M.,Inganas O.,Gustafsson G.,et al..Light-emitting-diodes with variable Colors from polymer blends[J].Nature,1994,372(6505):444-446
[150]Tu G.L.,Zhou Q.G.,Cheng Y.X.,et al..White electroluminescence from polyfluorene chemically doped with 1,8-napthalimide moieties[J].Appl.Phys.Lett.,2004,85(12):2172-2174.
[151]Xu Q.F.,Duong H.M.,Fred W.,et al..Efficient single-layer "twistacene"-doped polymer white light-emitting diodes[J].Appl.Phys.Lett.,2004,85(16):3357-3359
[152]朱明华编.仪器分析(第三版)[M].高等教育出版社,2000:275