酚类环境雌激素的色谱测定方法及其应用研究
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摘要
目的：选择酚类环境雌激素包括双酚A(BPA)、4-壬基酚(4-NP)、4-叔辛基酚(4-tOP)、4-叔丁基酚(4-tBP)、四溴双酚A(TBBPA)、己烯雌酚(DES)和内源性雌激素，α-和β-雌二醇等为研究对象，分别建立大鼠血清和组织中的双酚A和4-壬基酚的测定方法并用于它们的毒代动力学研究；水产品和食品包装材料中的双酚A、4-壬基酚等8多种环境雌激素的分析方法，为研究环境雌激素污染现状和评价环境雌激素对人体健康的影响提供技术手段和科学依据。
方法：优化了上述酚类环境雌激素在生物样品、水产品和食品包装材料样品中的前处理和测定条件，分别建立了高效液相色谱、气相色谱-质谱和毛细管电泳分析方法。
1．高效液相色谱-直接荧光法检测大鼠血清、肝和睾丸组织中双酚A和4-壬基酚 建立了大鼠血清、肝和睾丸组织中BPA和4-NP的高效液相色谱-直接荧光测定方法。大鼠血清经正己烷-乙醚混合溶剂(70：30，v／v)提取后，取有机相用氮气流吹干，残渣用流动相溶解定容后分析。对于大鼠肝、睾丸组织样品，采用乙酸-乙酸铵缓冲液匀浆，加甲醇超声萃取，用C18小柱净化后，进行高效液相色谱分析。色谱检测条件为：C18色谱柱，流动相为乙腈-乙酸铵缓冲液(pH4.5)，流速为1.0ml／min。荧光检测波长为
Objective: In order to provide sensitive and reliable technique for the study of the relationship between environmental estrogens and diseases, chromatographic analytical methods for three kinds of representative environmental estrogens such as industrial chemicals including bisphenol A (BPA), 4-nonylphenol(4-NP), 4-tert-octylphenol(4-tOP),
4-tert-butylphenol(4-tBP) and tetrabromobisphenol A(TBBPA), synthetic compounds used as growth promoters of farm animals ( i.e. diethylstilbestrol, DES) and natural estrogens (i.e. estradiol) in rat serum and tissues, aquatic products and food packing materials were to be developed, respectively.
方法：优化了上述酚类环境雌激素在生物样品、水产品和食品包装材料样品中的前处理和测定条件，分别建立了高效液相色谱、气相色谱-质谱和毛细管电泳分析方法。
1．高效液相色谱-直接荧光法检测大鼠血清、肝和睾丸组织中双酚A和4-壬基酚 建立了大鼠血清、肝和睾丸组织中BPA和4-NP的高效液相色谱-直接荧光测定方法。大鼠血清经正己烷-乙醚混合溶剂(70：30，v／v)提取后，取有机相用氮气流吹干，残渣用流动相溶解定容后分析。对于大鼠肝、睾丸组织样品，采用乙酸-乙酸铵缓冲液匀浆，加甲醇超声萃取，用C18小柱净化后，进行高效液相色谱分析。色谱检测条件为：C18色谱柱，流动相为乙腈-乙酸铵缓冲液(pH4.5)，流速为1.0ml／min。荧光检测波长为
Objective: In order to provide sensitive and reliable technique for the study of the relationship between environmental estrogens and diseases, chromatographic analytical methods for three kinds of representative environmental estrogens such as industrial chemicals including bisphenol A (BPA), 4-nonylphenol(4-NP), 4-tert-octylphenol(4-tOP),
4-tert-butylphenol(4-tBP) and tetrabromobisphenol A(TBBPA), synthetic compounds used as growth promoters of farm animals ( i.e. diethylstilbestrol, DES) and natural estrogens (i.e. estradiol) in rat serum and tissues, aquatic products and food packing materials were to be developed, respectively.
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