酞菁—二氧化硅纳米材料的制备与应用
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摘要
本论文共分为五章,包括绪论、四羧基铝酞菁纳米粒子、四羧基铁酞菁纳米粒子及多功能磁性二氧化硅纳米管的制备与应用和展望。
第一章为绪论,介绍了不断发展的纳米科技,对用作标记物的荧光纳米材料做了小结,着重讲述了二氧化硅纳米粒子的应用与合成,并对多功能纳米材料-超顺磁性二氧化硅纳米粒子和纳米管的应用做了简介,并在此基础上提出了本论文选题依据、研究目标、和研究内容。
第二章主要研究四羧基铝酞菁纳米粒子的制备与应用。本章分为两节,第一节主要通过四乙氧基硅烷在反向胶束构成的纳米水池中水解首次制备出非共价四羧基铝酞菁纳米粒子,该荧光纳米颗粒能用于指示溶液pH的变化。第二节主要通过四羧基铝酞菁修饰的硅烷前体和四乙氧基硅烷在反向胶束构成的纳米水池中共水解制备出共价四羧基铝酞菁纳米粒子。以这些荧光纳米粒子作为荧光探针,建立了一个灵敏的检测痕量人IgG的荧光免疫分析新方法。
第三章报道了四羧基铁酞菁纳米粒子的制备与应用。分为两节,第一节通过将四羧基铁酞菁共价包埋到纳米粒子中,制备四羧基铁酞菁-二氧化硅纳米粒子并用于硫胺素的测定。第二节通过将四羧基铁酞菁偶联到氨基化磁性二氧化硅纳米粒子的表面制备出磁性四羧基铁酞菁纳米粒子,并应用于催化水溶液中有机污染物的降解反应。
第四章初步探讨了利用模板法合成了内、外表面功能化的磁性二氧化硅纳米管的制备与应用。将四羧基铝酞菁与磁性二氧化硅纳米管相结合,制备出对pH敏感的磁性二氧化硅纳米管。四羧基铝酞菁分别共轭到磁性二氧化硅纳米管的内、外表面后,仍然保持了其水溶液的荧光强度随溶液的pH的增加而增强的特性,可以用于溶液体系中的pH值的检测。同时,更有为意义的是,结合其它表征手段,发现四羧基铝酞菁的性质并未发生改变,所以该方法制备的表面功能化磁性二氧化硅纳米管不仅可以用做pH值的检测,还可以用来作为新型纳米材料载体,在细胞标记、药物运输、DNA转染、选择性分离,或作为催化剂载体等方面大有用途。
第五章对下一步的研究工作提出了设想。
This dissertation consists of five chapters, including introduction, synthesis and application of tetra-substituted carboxyl aluminum phthalocyanine (AlC_4Pc)-silica nanoparticles, synthesis and applicantion of tetra-substituted carboxyl iron phthalocyanine(TCFePc)-silica nanoparticles, synthesis and applicantion of multifunctional magnetic silica nanotubes, and the conclusion and prospect of the present research work.
In chapter one, the progress and development of nanotechnology was introduced. The fluorescent nanomaterials which can be used as markers were summarized briefly. And how to synthsize and apply the silica nanoparticles was described in details. The research proposal for this dissertation was also presented.
In chapter two, the preparation and application of AlC_4Pc-silica nanoparticles were reported. This chapter was divided into two sections. The content of the first section was about using the microemulsion method to synthesize non-covalent fluorescent nanoparticles, AlC_4Pc-silica nanopartices. And the possibility of using the fluorescent nanoparticles as new fluorescent indicator for pH determination was also investigated. In the second section, covalent fluorescent nanoparticles were prepared by controlling the cohydrolysis of AlC_4Pc silylanization precursor and TEOS and APTEOS in W/O microemulsion. A fluoroimmunoassay method using the fluorescent nanoparticles was proposed for the determination of trace amount of IgG.
In chapter three, two different methods were used to synthesize the TCFePc catalyst-supported silica nanoparticles. In the first section, by controlling the cohydrolysis of TCFePc silylanization precursor and TEOS in W/O microemulsion, the TCFePc-silica nanoparticles were formed and used to highly sensitive determinate thiamine. In the second section, TCFePc were covalently attached to the surface amino-functionalized magentic silica nanoparticles to form the TCFePc-magnetic SiO_2 nanoparticles, which used to catalyze the degradation reaction of organic pollutants in water. Compared with free TCFePc, the magnetic supported-catalyst has the advantages of ready separation by external magnetic field and can be directly used for the next run.
The chapter four was about the preliminary investigation of the preparation and application of the surface-functionalized magnetic silica nanotubes. Combining AlC_4Pc with modified magnetic silica nanotubes which synthesized by alumina template membrane method, the AlC_4Pc-magnetic nanotubes were firstly synthesized and characterized. From the experimental results, the inner- or outer-AlC_4Pc magnetic silica nanotubes had the similar feature with free AlC_4Pc. These results indicated that the amino surface-functionalized magnetic silica nanotubes will be a promising platform for the applications of targeting drug delivery, DNA transfection, selective separation, catalyst carriers and so on.
In chapter five, the final part of the dissertation, the prospect of this research was discussed.
第一章为绪论,介绍了不断发展的纳米科技,对用作标记物的荧光纳米材料做了小结,着重讲述了二氧化硅纳米粒子的应用与合成,并对多功能纳米材料-超顺磁性二氧化硅纳米粒子和纳米管的应用做了简介,并在此基础上提出了本论文选题依据、研究目标、和研究内容。
第二章主要研究四羧基铝酞菁纳米粒子的制备与应用。本章分为两节,第一节主要通过四乙氧基硅烷在反向胶束构成的纳米水池中水解首次制备出非共价四羧基铝酞菁纳米粒子,该荧光纳米颗粒能用于指示溶液pH的变化。第二节主要通过四羧基铝酞菁修饰的硅烷前体和四乙氧基硅烷在反向胶束构成的纳米水池中共水解制备出共价四羧基铝酞菁纳米粒子。以这些荧光纳米粒子作为荧光探针,建立了一个灵敏的检测痕量人IgG的荧光免疫分析新方法。
第三章报道了四羧基铁酞菁纳米粒子的制备与应用。分为两节,第一节通过将四羧基铁酞菁共价包埋到纳米粒子中,制备四羧基铁酞菁-二氧化硅纳米粒子并用于硫胺素的测定。第二节通过将四羧基铁酞菁偶联到氨基化磁性二氧化硅纳米粒子的表面制备出磁性四羧基铁酞菁纳米粒子,并应用于催化水溶液中有机污染物的降解反应。
第四章初步探讨了利用模板法合成了内、外表面功能化的磁性二氧化硅纳米管的制备与应用。将四羧基铝酞菁与磁性二氧化硅纳米管相结合,制备出对pH敏感的磁性二氧化硅纳米管。四羧基铝酞菁分别共轭到磁性二氧化硅纳米管的内、外表面后,仍然保持了其水溶液的荧光强度随溶液的pH的增加而增强的特性,可以用于溶液体系中的pH值的检测。同时,更有为意义的是,结合其它表征手段,发现四羧基铝酞菁的性质并未发生改变,所以该方法制备的表面功能化磁性二氧化硅纳米管不仅可以用做pH值的检测,还可以用来作为新型纳米材料载体,在细胞标记、药物运输、DNA转染、选择性分离,或作为催化剂载体等方面大有用途。
第五章对下一步的研究工作提出了设想。
This dissertation consists of five chapters, including introduction, synthesis and application of tetra-substituted carboxyl aluminum phthalocyanine (AlC_4Pc)-silica nanoparticles, synthesis and applicantion of tetra-substituted carboxyl iron phthalocyanine(TCFePc)-silica nanoparticles, synthesis and applicantion of multifunctional magnetic silica nanotubes, and the conclusion and prospect of the present research work.
In chapter one, the progress and development of nanotechnology was introduced. The fluorescent nanomaterials which can be used as markers were summarized briefly. And how to synthsize and apply the silica nanoparticles was described in details. The research proposal for this dissertation was also presented.
In chapter two, the preparation and application of AlC_4Pc-silica nanoparticles were reported. This chapter was divided into two sections. The content of the first section was about using the microemulsion method to synthesize non-covalent fluorescent nanoparticles, AlC_4Pc-silica nanopartices. And the possibility of using the fluorescent nanoparticles as new fluorescent indicator for pH determination was also investigated. In the second section, covalent fluorescent nanoparticles were prepared by controlling the cohydrolysis of AlC_4Pc silylanization precursor and TEOS and APTEOS in W/O microemulsion. A fluoroimmunoassay method using the fluorescent nanoparticles was proposed for the determination of trace amount of IgG.
In chapter three, two different methods were used to synthesize the TCFePc catalyst-supported silica nanoparticles. In the first section, by controlling the cohydrolysis of TCFePc silylanization precursor and TEOS in W/O microemulsion, the TCFePc-silica nanoparticles were formed and used to highly sensitive determinate thiamine. In the second section, TCFePc were covalently attached to the surface amino-functionalized magentic silica nanoparticles to form the TCFePc-magnetic SiO_2 nanoparticles, which used to catalyze the degradation reaction of organic pollutants in water. Compared with free TCFePc, the magnetic supported-catalyst has the advantages of ready separation by external magnetic field and can be directly used for the next run.
The chapter four was about the preliminary investigation of the preparation and application of the surface-functionalized magnetic silica nanotubes. Combining AlC_4Pc with modified magnetic silica nanotubes which synthesized by alumina template membrane method, the AlC_4Pc-magnetic nanotubes were firstly synthesized and characterized. From the experimental results, the inner- or outer-AlC_4Pc magnetic silica nanotubes had the similar feature with free AlC_4Pc. These results indicated that the amino surface-functionalized magnetic silica nanotubes will be a promising platform for the applications of targeting drug delivery, DNA transfection, selective separation, catalyst carriers and so on.
In chapter five, the final part of the dissertation, the prospect of this research was discussed.
引文
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