摘要
二硫化钼因具有催化效率高、稳定性好、层结构易于剥离拆分等优点,成为继石墨烯研究热潮后的又一代表性二维材料。材料的结构影响其性能,因此利用简单的方法制备结构独特和形貌均一的二硫化钼材料成为近年来材料学领域研究的热点之一。二硫化钼材料的制备方法包括物理法和化学法,重点介绍了利用化学法制备各种形貌二硫化钼材料。
Molybdenum disulfide(MoS_2),as a typical two-dimensional material with advantages including high catalytic efficiency,excellent stability and easy exfoliation,has become a new study following the graphene.The structures could have great effect on their performance,producing MoS_2 with novel structures and well-definedmorphologies by simple methods therefore became a hotresearch in the fields of materials science,recently.The synthesis methods of MoS_2 included physical method and chemical method.MoS_2 with diverse morphologies produced by chemical methodswere mainly introduced.
引文
[1]马浩,杨瑞霞,李春静.层状二硫化钼材料的制备和应用进展[J].材料导报,2017,31(3):7-14.
[2] Wang H D,Xu B S,Liu J J,et al.Characterization and anti-friction on the solid lubrication MoS2film prepared by chemical reaction technique[J].Science&Technology of Advanced Materials,2008,6(5):535-539.
[3] Zhang S,Zeng Y W,Wang Z T,et al.Glycerol-controlled synthesis of MoS2hierarchical architectures with well-tailored subunits and enhanced electrochemical performance for lithium ion batteries[J].Chemical Engineering Journal,2018,334:487-496.
[4] Anwar T,Wang L,Sagar R U R,et al.Molybdenum disulfide grafted titania nanotube arrays as high capacity retention anode material for lithium ion batteries[J].Applied Nanoscience,2017,7(1/2):67-73.
[5] Deng Y,Li J,Li T et al.Life cycle assessment of high capacity molybdenum disulfide lithium-ion battery for electric vehicles[J].Energy,2017,123:77-88.
[6] Guo B J,Feng Y,Chen X F,et al.Preparation of yolk-shell MoS2nanospheres covered with carbon shell for excellent lithium-ion battery anodes[J].Applied Surface Science,2017,434:1021-1029.
[7] He P G,Zhao K R,Huang B Y,et al.Mechanically robust and sizecontrolled MoS2/graphene hybrid aerogels as high-performance anodes for lithium-ion batteries[J].Journal of Materials Science,2018,53(6):4482-4493.
[8] Xiao H Q,Wang S T,Zhang S,et al.Interlayer expanded molybdenum disulfide nanosheets assembly for electrochemical supercapacitor with enhanced performance[J].Materials Chemistry&Physics,2017,192:100-107.
[9] Alamro T,Ram M K.Polyethylenedioxythiophene and molybdenum disulfide nanocomposite electrodes for supercapacitor applications[J].Electrochimica Acta,2017,235:623-631.
[10] Fang L X,Qiu Y,Li W,et al.Three-dimensional flower-like MoS2-Co Se2heterostructure for high performance supercapacitors[J].J.Colloid Interface Sci.,2017,512:282-290.
[11] Liu Y R,Hu K H,Hu E Z,et al.Double hollow MoS2nano-spheres:Synthesis,tribological properties,and functional conversion from lubrication to photocatalysis[J].Applied Surface Science,2017,392:1144-1152.
[12] Quinn M D J,Ho H,Notley S M.Aqueous dispersions of exfoliated molybdenum disulfide for use in visible-light photocatalysis[J].Applied Materials&Interfaces,2013,5(23):12751-12756.
[13]王毅,李刚,李朋伟,等.层状二硫化钼光催化产氢的研究进展[J].半导体光电,2016,37(4):461-466.
[14] Guo G H,Hong J H,Cong C J,et al.Molybdenum disulfide synthesized by hydrothermal method as anode for lithium rechargeable batteries[J].Journal of Materials Science,2005,40(9/10):2557-2559.
[15] Wang J,Wang P Y,Wang H H,et al.Preparation of molybdenum disulfide coated Mg/Al layered double hydroxide composites for efficient removal of chromium(Ⅵ)[J].Acs Sustainable Chemistry&Engineering,2017,5(8):7165-7174.
[16] Zhang D Z,Sun Y E,Jiang C X,et al.Room temperature hydrogen gas sensor based on palladium decorated tin oxide/molybdenum disulfide ternary hybrid via hydrothermal route[J].Sensors&Actuators B Chemical,2017,242:15-24.
[17] Li D,Li Jianwei,Han C Q,et al.Few-layered MoS2nanostructures for highly efficient visible light photocatalysis[J].Nano,2016,11(10):70-76.
[18] Yu D B,Feng Y,Zhu Y F,et al.Template synthesis and characterization of molybdenum disulfide nanotubules[J].Materials Research Bulletin,2011,46(9):1504-1509.
[19] Kadiev K M,Khadzhiev S N,Kadieva M Kh,et al.Ex situ synthesis of sulfided molybdenum-containing ultrafine hydroconversion catalysts[J].Petroleum Chemistry,2017,57(7):608-617.
[20] Wang X,Xing W Y,Feng X M,et al.Enhanced mechanical and barrier properties of polyurethane nanocomposite films with randomly distributed molybdenum disulfide nanosheets[J]. Composites Science&Technology,2016,127:142-148.
[21] Wang N,Wei F,Qi Y H,et al.Synthesis of strongly fluorescent molybdenum disulfide nanosheets for cell-targeted labeling[J].Acs Applied Materials&Interfaces,2014,6(22):19888-19894.
[22] Ortiz-Quiles E O,Cabrera C R.Exfoliated molybdenum disulfide for dye sensitized solar cells[J].Flatchem,2017,2:1-7.
[23] Kim J,Kim J S,Kim T,et al.Phase conversion of chemically exfoliated molybdenum disulfide[J].Current Applied Physics,2017,17(1):60-65.
[24] Wang T L,Zhao G,Sun C L,et al.Graphene-assisted exfoliation of molybdenum disulfide to fabricate 2D heterostructure for enhancing lithium storage[J].Advanced Materials Interfaces,2017,4(14):1601187.
[25] Kwieci觡ski W,Sotthewes K,Poelsema B et al.Chemical vapor deposition growth of bilayer graphene in between molybdenum disulfide sheets[J].Journal of Colloid&Interface Science,2017,505:776-782.
[26] Dankert A,Pashaei P,Kamalakar M V,et al.Spin-polarized tunneling through chemical vapor deposited multilayer molybdenum disulfide[J].Acs Nano,2017,11(6):6389-6395.
[27] Elibol K,Susi T,O′Brien M,et al.Grain boundary-mediated nanopores in molybdenum disulfide grown by chemical vapor deposition[J].Nanoscale,2016,9(4):1591-1598.
[28] Aleksandrov S E,Filatov K D,Tyurikov K S.Synthesis of molybdenum disulfide particles by aerosol-assisted chemical vapor deposition[J].Russian Journal of Applied Chemistry,2016,89(5):714-718.
[29] Yang Z F,Grassi R,Freitag M,et al.Spatial/temporal photocurrent and electronic transport in monolayer molybdenum disulfide grown by chemical vapor deposition[J].Applied Physics Letters,2016,108(8):147.
[30] Wang X J,Wu Q,Jiang K L,et al.One-step synthesis of water-soluble and highly fluorescent MoS2quantum dots for detection of hydrogen peroxide and glucose[J].Sensors&Actuators B Chemical,2017,252:183-190.
[31]许献云.MoS2纳米线的制备和显微分析[J].安徽化工,2005,31(3):39-40.
[32]李方,高玉伟,张志毅,等.水热法合成二硫化钼花状微球及其电容性能研究[J].功能材料,2017,48(3):3145-3148.
[33]武子茂,兰会林.水热法制备不同形貌二硫化钼及其电化学电容性能[J].兰州理工大学学报,2016,42(5):18-22.
[34] Zhang H,Cong L,Wang J X,et al.Impact of CTAB on morphology and electrochemical performance of MoS2nanoflowers with improved lithium storage properties[J].Journal of Materials Science Materials in Electronics,2018,29(5):3631-3639.
[35]周军,兰新哲,张秋利,等.微乳液法制备纳米二硫化钼酸沉过程研究[J].有色金属:冶炼部分,2011(8):47-51.
[36] Li Y G,Wang H L,Xie L M,et al.MoS2nanoparticles grown on graphene:An advanced catalyst for the hydrogen evolution reaction[J].Journal of the American Chemical Society,2011,133(19):7296-7299.
[37] Tang G G,Sun J R,Chen W,et al.Surfactant-assisted hydrothermal synthesis and tribological properties of flower-like MoS2nanostructures[J].Micro&Nano Letters,2013,8(3):164-168.
[38] Zhu Y D,Feng Y,Yu D B,et al.Synthesis of MoS2nanotubule arrays by aluminum oxide template[J].Rare Metal Materials&Engineering,2011,40(4):339-341.
[39] Wang Z Y,Li H,Liu Z,et al.Mixed low-dimensional nanomaterial:2D ultranarrow MoS2inorganic nanoribbons encapsulated in quasi-1D carbon nanotubes[J].Journal of the American Chemical Society,2010,132(39):13840-13847.
[40]王跃峰,赵鹏,曾一,等.化学气相沉积法制备富勒烯结构二硫化钼纳米粒子[J].应用化工,2008,37(12):1413-1415,1418.
[41] Feldman Y,Wasserman E,Srolovitz D J,et al.High-rate,gas-phase growth of MoS2nested inorganic fullerenes and nanotubes[J].Science,1995,267(5195):222-225.
[42] Liu H,Si M W,Najmaei S,et al.Statistical study of deep submicron dual-gated field-effect transistors on monolayer chemical vapor deposition molybdenum disulfide films[J].Nano Letters,2013,13(6):2640-2646.
[43] Hu D,Xiang J,Zhou Q W,et al.One-step chemical vapor deposition of MoS2nanosheets on sinws as photocathodes for efficient and stable solar-driven hydrogen production[J].Nanoscale,2018,10(7):3518-3525.
[44] Xu W S,Li S,Zhou S,et al.Large dendritic monolayer MoS2grown by atmospheric pressure chemical vapor deposition for electrocatalysis[J].ACS Appl Mater Interfaces,2018,10(5):4630-4639.
[45] Ambrosi A,Sofer Z,Pumera M.Molybdenum disulfide:Lithium intercalation compound dramatically influences the electrochemical properties of exfoliated MoS2(small 5/2015)[J].Small,2015,11(5):605-612.
[46] Fan X B,Xu P T,Zhou D K,et al.Fast and efficient preparation of exfoliated 2H MoS2nanosheets by sonication-assisted lithium intercalation and infrared laser-induced 1T to 2H phase reversion[J].Nano Letters,2015,15(9):5956-5960.
[47] Eda G,Yamaguchi H,Voiry D,et al.Photoluminescence from chemically exfoliated MoS2[J].Nano Letters,2011,11(12):5111-5116.
[48]马少华,杨鹏.油溶性二硫化钼纳米微粒的制备及抗磨性能[J].合成材料老化与应用,2015(1):52-54,121.
[49] Vattikuti S V P,Byon Chan,Reddy C V,et al.Co-precipitation synthesis and characterization of faceted MoS2nanorods with controllable morphologies[J].Applied Physics A,2015,119(3):813-823.
[50] Yu H T,Liu Y,Brock S L.Synthesis of discrete and dispersible MoS2nanocrystals[J].Inorganic Chemistry,2008,47(5):1428-1434.
[51]邵红红,陈威.射频磁控溅射法制备二硫化钼薄膜[J].润滑与密封,2007,32(12):43-46.
[52]沈志刚,李金芝,易敏,等.一种射流空化技术制备二维纳米二硫化钼的方法:中国,102398920A[P].2012-04-04.
[53] Kong D S,Wang H T,Cha J J,et al.Synthesis of MoS2and MoSe2films with vertically aligned layers[J].Nano Letters,2013,13(3):1341-1347.
[54]谢绵钰,谌冰,乐松.纳米片状MoS2的固态杂化微波合成[J].人工晶体学报,2015,44(5):1394-1397.
[55] Li Y W,Yin X L,Wu W.Preparation of few-layer MoS2nanosheets via an efficient shearing exfoliation method[J].Industrial&Engineering Chemistry Research,2018,57(8):2838-2846.