摘要
采用SPME-GC/MS联用技术分析山胡椒果实挥发性成分,共分离出57个化学成分,其中匹配度大于等于80%的化合物有45种,占果实挥发性物质含量的78.94%。其中柠檬醛、石竹烯和(Z)-3,7-二甲基-2,6-辛二烯醛是含量最高的三种物质,相对含量为分别为23.09%、22.04%、17.23%,占整个挥发性物质的62.36%。
Analyzed by GC/MS,57 main volatile matter were separated and identified using SPME from fruit of spicebush. 45 compounds were identified, matching degree is greater than or equal to 80%, which accounts for 78.94% of the total content of volatile matter. Citral, caryophyllene and 2,6-Octadienal, 3,7-dimethyl-,(Z)-were the highest levels in the whole volatile matter, which relative content was 23.09%, 22.04% and 23.09% respectively, and accounts for 62.36% of the total content of volatile matter.
引文
[1]张朝凤,王峥涛.山胡椒属药用植物的研究进展[J].沈阳药科大学学报,2000,17(3):230-234.
[2]陈随波,左艇.河南山胡椒属植物资源及其药理、化学及应用研究[J].河南中医学院学报,2005,118(20):25-27.
[3]卢艳花,魏东芝,蒋晓萌.中药有效成分提取分离技术[M].北京:化学工业出版社,2005:8-350.
[4]赵利琴.山胡椒属萜类及其生物活性研究进展[J].时珍国医国药,2006,17(2):171-174.
[5]赵奇志,赵毅民,王克军.狭叶山胡椒根中的生物碱成分[J].药学学报,2005,40(10):931-934.
[6]张小云,覃文庆,喻连香.山胡椒挥发油的提取及其抑菌活性研究[J].现代生物医学进展,2010(1):133-136.
[7]潘晓军,林观样,王贤亲,等.浙产山胡椒根挥发油化学成分的研究[J].光谱实验室,2010(5):1777-1779.
[8]郭凤领,吴金平,矫振彪,等.顶空固相微萃取气质联用检测高山根韭菜挥发性风味物质[J].长江蔬菜,2017(6):25-28.[8]KALA C P.Ethnomedicinal botany of the Apatani in the Eastern Himalayan region of India[J].J of Ethnobiology and Ethnomedicine,2005,1(11):1-8.
[9]游玉明,黄琳琳.山胡椒提取物的抑菌活性及其稳定性[J].食品与发酵工业,2013(5):116-119.
[10]李芳,游玉明.山胡椒成熟过程中挥发油成分的变化[J].中国调味品,2016(4):66-69.