回潮温度对中试试样烟丝中致香物质的影响
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摘要
以中国市售具有代表性的主力卷烟品牌M的两个不同批次(A、B)样品为原料,建立了静态顶空-GC/MS联用法,MES自动控制系统采集数据,对A、B两批次烟丝样品中的致香成分进行测定。结果显示:(1)两个批次的成品烟丝共检测出40种核心致香成分,其中批次A含34种,批次B含37种;(2) 3-甲基-1-丁醇、2,6-二甲基吡嗪、正十六烷、2-乙酰基呋喃、2-己烯-1-醇、顺式-4-庚烯醛为A中未检出的成分,2-甲基吡嗪、异戊烯醇、2-乙酰基吡咯为B中未检出的成分;(3) B中的致香物质相对总含量小于样品A中的致香物质相对总含量,将回潮区温度控制在60℃有利于保留烟丝中的致香成分。
Taking two different representative batches(A,B)of the domestic commercial cigarette brand M as raw materials.A static headspace-GC/MS method was established and the datas were collected by the MES automatic control system.Aroma components in two batches of tobacco samples(A and B)were determined.RESULTS A total of 40 core aroma components were detected in two batches of finished cut tobacco,of which batch A contained 34 and batch B contained 37;3-methyl-1-butanol,2,6-dimethyl Pyridazine,n-hexadecane,2-acetylfuran,2-hexen-1-ol,cis-4-heptenal are undetected components in A,2-methylpyrazine, isoprene Enol and 2-acetylpyrrole were undetected components in B;the relative total content of aroma substances in B was less than that of aroma substances in sample A,and controlling the temperature of the regain zone at 60 ℃was favorable to retain the aroma components in the tobacco.
Taking two different representative batches(A,B)of the domestic commercial cigarette brand M as raw materials.A static headspace-GC/MS method was established and the datas were collected by the MES automatic control system.Aroma components in two batches of tobacco samples(A and B)were determined.RESULTS A total of 40 core aroma components were detected in two batches of finished cut tobacco,of which batch A contained 34 and batch B contained 37;3-methyl-1-butanol,2,6-dimethyl Pyridazine,n-hexadecane,2-acetylfuran,2-hexen-1-ol,cis-4-heptenal are undetected components in A,2-methylpyrazine, isoprene Enol and 2-acetylpyrrole were undetected components in B;the relative total content of aroma substances in B was less than that of aroma substances in sample A,and controlling the temperature of the regain zone at 60 ℃was favorable to retain the aroma components in the tobacco.
引文
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[12]陆冰琳,黄世杰,朱静.静态顶空-气质联用仪对铁观音茶叶中挥发性香味成分的分析[J].园艺与种苗,2015(8):78-79.
[13]员梦梦,李保印,周秀梅.静态顶空进样-气质联用法测定玫瑰花香成分[J].分析检测,2016,37(20):101-109.
[14]蒋举兴,夏启东,段焰青,等.卷烟香精香料中23种加香物质的气相色谱质谱法检测[J].食品工业,2013,34(9):221-223.
[15]李孟华,徐玉琼,张峻松.烟草中烟碱的分析研究进展[J].农产品加工:学刊,2009(9):71-74.
[2]景延秋,宫长荣,张月华,等.烟草香味物质分析研究进展[J].中国烟草科学,2005,26(2):44-48.
[3]段胜智,李军营,杨利云,等.烟叶致香成分及其环境影响因子的研究进展[J].贵州农业科学,2015,43(1):45-52.
[4]刘字,颜合洪.烟叶致香物质的研究进展[J].作物研究所,2006,20(5):470-474.
[5]SCHUMACHER J N,VESTAL L.Isolation and identification of some components of Turkish tobacco[J].Tob Sci,1974(18):43-48.
[6]黄学跃,柴家荣.两个晒烟品种主要致香成分分析[J].云南农业大学学报,2006,21(2):192-195.
[7]谢剑平,赵明月,吴鸣.白肋烟重要香味物质组成的研究[J].烟草科技,2002(10):3-16.
[8]曹琳,秦利霞,康诗钊,等.香精香料的常见检测方法综述[J].上海应用技术大学,2017,45(21):17-20.
[9]黄曼艳,陈森林,陶红,等.烟叶中致香成分前处理与检测方法研究进展[J].食品安全质量检测学报,2018,9(9):2 072-2 079.
[10]覃光炯,饶雄飞,杨艳华,等.静态顶空-气质联用法分析烤烟中香味物质[J].广州化工,2015,43(11):116-118.
[11]卢斌斌,张璟琳,曾世通,等.静态顶空-GC/MS技术分析浸膏中的溶剂残留[J].烟草科技,2016,49(10):60-65.
[12]陆冰琳,黄世杰,朱静.静态顶空-气质联用仪对铁观音茶叶中挥发性香味成分的分析[J].园艺与种苗,2015(8):78-79.
[13]员梦梦,李保印,周秀梅.静态顶空进样-气质联用法测定玫瑰花香成分[J].分析检测,2016,37(20):101-109.
[14]蒋举兴,夏启东,段焰青,等.卷烟香精香料中23种加香物质的气相色谱质谱法检测[J].食品工业,2013,34(9):221-223.
[15]李孟华,徐玉琼,张峻松.烟草中烟碱的分析研究进展[J].农产品加工:学刊,2009(9):71-74.