Synthesis of New 3-(Furan-2-yl)-Substituted Dibenzo-Diazepin-1-one Derivatives

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• 作者：Fang-Ming Wang ; Dan Bao ; Ming Wang ; Qing-Huan Yin ; Li-Zhuang Chen and Guang-Fan Han
• 刊名：Journal of Heterocyclic Chemistry
• 出版年：2016
• 出版时间：July 2016
• 年：2016
• 卷：53
• 期：4
• 页码：1081-1085
• 全文大小：379K
• ISSN：1943-5193

文摘

A new series of 3-(furan-2-yl) dibenzo-diazepin-1-one derivatives were synthesized by condensation of pan class="TH_term3">5-(furan-2-yl)-1,3-cyclohexanedionepan>, pan class="TH_term3">o-phenylenediaminepan>, and aromatic aldehydes, in which in some of them existed two very close isomer compounds. All the compounds were characterized by IR, MS, ¹H NMR, and elemental analysis. Also presented were the crystal structures of , and , which were obtained and determined by X-ray single-crystal diffraction.