CNTs/CaIn2S4 (CIS) composites were prepared by a microwave hydrothermal method.
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CNTs were embedded tightly in the hierarchical marigold-like CIS microspheres.
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Intimate contact between CNTs and CIS made interfacial charge transfer available.
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The composite exhibited obviously higher photocatalytic activity than bare CIS.
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The composite was applicable in both environment remediation and energy conversion.
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