Different sample treatments for the determination of ICM-XR in fish samples followed by LC-HRMS

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• 作者：Mireia Nú ; ñ ; ez ; Francesc Borrull ; Nú ; ria Fontanals ; ^{nuria.fontanals@urv.cat} ; Eva Pocurull
• 关键词：Iodinated X-ray contrast media ; Pressurised liquid extraction ; High resolution mass spectrometry ; Matrix effect ; Fish samples
• 刊名：Talanta
• 出版年：2017
• 出版时间：15 January 2017
• 年：2017
• 卷：163
• 期：Complete
• 页码：1-7
• 全文大小：325 K
• 卷排序：163

文摘

First PLE/SPE/LC-HRMS method to determine a group of (ICM-XR). Different clean-up strategies were evaluated in order to reduce the high ME. The Oasis® MCX sorbent in the SPE was employed in order to retain interferences. The method was validated in different fish species according to their % lipid content.