Mechanism of the self-condensation of GlcNH<sub>2</sub>: insights from in situ NMR spectroscopy and DFT study

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Mechanism of the self-condensation of GlcNH₂: insights from in situ NMR spectroscopy and DFT study

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作者：Lingyu Jia^a ; ^b ; Xingchen Liu^c ; Yan Qiao^c ; Christian Marcus Pedersen^d ; Zhenzhou Zhang^b ; ^c ; Hui Ge^a ; Zhihong Wei^c ; Yanyan Chen^c ; Xiaodong Wen^c ; Xianglin Hou^a ; ^{houxl@sxicc.ac.cn" class="auth_mail" title="E-mail the corresponding author} ; Yingxiong Wang^a ; ^{wangyx@sxicc.ac.cn" class="auth_mail" title="E-mail the corresponding author}
关键词：in situ NMR ; DFT calculations ; Reaction mechanism ; Chitin biomass
刊名：Applied Catalysis B: Environmental
出版年：2017
出版时间：March 2017
年：2017
卷：202
期：Complete
页码：420-429
全文大小：2943 K

文摘

class="label">•: In situ NMR combined with ESI-MS spectrometry was applied to investigate reaction mechanism.
class="label">•: Isotopic-labelling experiments disclose that there are two parallel pathways open to the intermediate dihydrofructosazine.
class="label">•: DFT calculation indicates that [C₂C₁Im][OAc] is an acid-base dual activation catalyst in catalyzing DOF and FZ formation.

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