Tetragonal β-In2S3: Partial ordering of In3 + vacancy and visible-light photocatalytic activities in both water and nitrate reduction
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A highly crystallized tetragonal β-In2S3 exhibits a partial ordering of In3 + vacancy.

It contained flower-like spherical particles, further composed of very thin petals.

Tetragonal β-In2S3 has an intrinsic photocatalytic water reduction activity.

The optimal H2 evolution rate was 442 μmol/h/g under pure visible light irradiation.

Nitrate conversion rate achieved 3.26 mg N/h under the irradiation of a Xe lamp.

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