“Non-hydrolytic” sol-gel synthesis of molybdenum sulfides
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Molybdenum sulfides were prepared by non-hydrolytic sol–gel chemistry.

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Nanocrystalline 3R-MoS2 and 2H-MoS2, and microcrystalline Mo2S3 were obtained.

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Particle morphology correlated strongly with crystalline phases.

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Ultrathin platelets with limited tendency to agglomerate were recovered.

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