Urea-formaldehyde monolithic column for hydrophilic in-tube solid-phase microextraction of aminoglycosides

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• 作者：Jiabin Wang^a ; ^{jbwang@fzu.edu.cn} ; ^{wangjb_1@163.com} ; Qi Zhao^a ; Nan Jiang^a ; Wenbang Li^a ; Li Chen^a ; Xucong Lin^b ; Zenghong Xie^b ; Lijun You^a ; Qiqing Zhang^a ; ^c ; ^{zhangqiq@126.com}
• 关键词：Aminoglycosides ; Evaporative light scattering detector ; Hydrophilic interaction ; In-tube solid-phase microextraction ; Urea-formaldehyde monolithic column
• 刊名：Journal of Chromatography A
• 出版年：2017
• 出版时间：17 February 2017
• 年：2017
• 卷：1485
• 期：Complete
• 页码：24-31
• 全文大小：1936 K
• 卷排序：1485

文摘

A urea-formaldehyde monolithic column was prepared for hydrophilic in-tube SPME of aminoglycosides. A sensitive method based on in-tube SPME-HPLC-ELSD was developed for determination of aminoglycosides. Short time-consuming, low disturbance and high detection sensitivity for the analytes were achieved.