Role of HPB in electrodeposition of Ni-Al2O3 coatings was studied systematically.
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Zeta potentials of the particles were measured in both Watt's bath and water.
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Dispersibility of particles is improved dynamically in Watt's bath with agitation.
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Co-deposition of Al2O3 particles is enhanced by cathode capture with HPB addition.
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Surfactants facilitate a smooth and dense coating by improving wetting of bath.
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