REE chemistry and mineralogy were examined on the Hercynian Liberty Hill pluton. The pluton is in the highly weathered and slowly eroding South Carolina Piedmont. In one profile, ion-adsorbed REE + Y ranged up to 581 mg/kg and were 77% of bulk REE + Y. In other profiles, ion-adsorbed REE + Y ranged 8–194 mg/kg and were 3–39% of bulk REE + Y. Low P content and hydrothermal alteration caused the high ion-adsorbed REE content.
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