Determination of “new psychoactive substances‿in postmortem matrices using microwave derivatization and gas chromatography-mass spectrometry

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Determination of “new psychoactive substances‿in postmortem matrices using microwave derivatization and gas chromatography-mass spectrometry

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作者：Clá ; udia Margalho^a ; ^{claudia.i.margalho@inmlcf.mj.pt" class="auth_mail" title="E-mail the corresponding author} ; ^{claudiamargalho@iol.pt" class="auth_mail" title="E-mail the corresponding author} ; Alice Castanheira^a ; Francisco Corte Real^a ; ^b ; Eugenia Gallardo^c ; Manuel Ló ; pez-Rivadulla^d
关键词：Cathinones ; Phenethylamines ; Alternative biological matrices ; Microwave fast derivatization ; Gas chromatography&ndash ; mass spectrometry
刊名：Journal of Chromatography B, Analytical Technologies in the Biomedical and Life Sciences
出版年：2016
出版时间：1 May 2016
年：2016
卷：1020
期：Complete
页码：14-23
全文大小：544 K

文摘

•: Determination, for the first time, of NPS in vitreous humor and pericardial fluid.
•: Good LOD using 100 μL of vitreous humor and 250 μL of pericardial fluid and blood.
•: A simple and sensible methodology with a microwave fast derivatization procedure.

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