Oxidative-addition of the N-H bond of saccharin (sacH) to a triosmium centre: Synthesis, structure and reactivity of Os<sub>3</sub>(CO)<sub>10</sub>(μ-H)(μ-sac)

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Oxidative-addition of the N-H bond of saccharin (sacH) to a triosmium centre: Synthesis, structure and reactivity of Os₃(CO)₁₀(μ-H)(μ-sac)

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作者：Shirajum Monira^a ; Sadiya Afrin^a ; Kazi A. Azam^a ; ^{kazi.ali.azam@gmail.com" class="auth_mail" title="E-mail the corresponding author} ; Md Kamal Hossain^a ; Derek A. Tocher^b ; Shishir Ghosh^a ; Subas Rajbangshi^a ; Shariff E. Kabir^a ; Graeme Hogarth^c ; ^{graeme.hogarth@kcl.ac.uk" class="auth_mail" title="E-mail the corresponding author}
关键词：Triosmium clusters ; Carbonyls ; Saccharin ; N&ndash ; H bond activation ; X-ray structures
刊名：Journal of Organometallic Chemistry
出版年：2015
出版时间：15 December 2015
年：2015
卷：799-800
期：Complete
页码：281-290
全文大小：991 K

文摘

•: Oxidative-addition of the N–H bond of saccharin to a triosmium cluster.
•: Reaction of Os₃(CO)_10-n(NCMe)_n (n = 1, 2) with saccharin.
•: Synthesis and structure of Os₃(CO)₁₀(μ-H) (μ-sac).
•: Reactions of Os₃(CO)₁₀(μ-H) (μ-sac) with PR₃ (R = Ph, Th, Fu).

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