SnF<sub>2</sub>-catalyzed glycerol ketalization: A friendly environmentally process to synthesize solketal at room temperature over on solid and reusable Lewis acid

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SnF₂-catalyzed glycerol ketalization: A friendly environmentally process to synthesize solketal at room temperature over on solid and reusable Lewis acid

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作者：Má ; rcio José ; da Silva ; ^{silvamj2003@ufv.br" class="auth_mail" title="E-mail the corresponding author} ; Fabio de Á ; vila Rodrigues ; Armanda Aparecida Jú ; lio
关键词：Tin(II) fluoride ; Glycerol ; Solketal ; Bioadditives ; Solvent-free process
刊名：Chemical Engineering Journal
出版年：2017
出版时间：1 January 2017
年：2017
卷：307
期：Complete
页码：828-835
全文大小：884 K

文摘

•: A solid SnF₂-catalyzed process produced solketal from glycerol at room temperature.
•: SnF₂ catalyst was easily recovered and reused without loss activity.
•: A process flow diagram with the best operating conditions was described.
•: A mechanism for solid SnF₂-catalyzed solketal synthesis was proposed.
•: SnF₂ operate in biphasic conditions with low proportion of glycerol to ketone.

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