Microwave-assisted enzymatic hydrolysis followed by extraction with restricted access nanocomposites for rapid analysis of glucocorticoids residues in liver tissue

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Microwave-assisted enzymatic hydrolysis followed by extraction with restricted access nanocomposites for rapid analysis of glucocorticoids residues in liver tissue

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作者：Jianan Feng^a ; ¹ ; Xiaodan Liu^a ; ^b ; ¹ ; Yan Li^a ; ^{yanli@fudan.edu.cn" class="auth_mail" title="E-mail the corresponding author} ; Gengli Duan^a
关键词：Microwave-assisted ; Enzymatic hydrolysis ; Graphene@mSiO2-C8 ; Glucocorticoids ; Liver ; Liquid chromatography-tandem mass spectrometry (LC-MS/MS)
刊名：Talanta
出版年：2016
出版时间：1 October 2016
年：2016
卷：159
期：Complete
页码：155-162
全文大小：1399 K

文摘

•: Microwave-assisted enzymatic hydrolysis and RAM-SPE were combined.
•: C8-functionalized hydrophobic interior pore-walls for extraction of glucocorticoids.
•: Different enzymatic hydrolysis influencing factors were optimized.
•: Different extraction conditions were optimized.

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