A simple, accurate, time-saving and green method for the determination of 15 sulfonamides and metabolites in serum samples by ultra-high performance supercritical fluid chromatography

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A simple, accurate, time-saving and green method for the determination of 15 sulfonamides and metabolites in serum samples by ultra-high performance supercritical fluid chromatography

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作者：Yuan Zhang^a ; ^b ; ^{13840149878@163.com" class="auth_mail" title="E-mail the corresponding author} ; Wei-E Zhou^a ; Shao-Hui Li^a ; Zhi-Qin Ren^a ; Wei-Qing Li^a ; Yu Zhou^b ; Xue-Song Feng^b ; Wen-Jie Wu^a ; Feng Zhang^a ; ^{fengzhang@126.com" class="auth_mail" title="E-mail the corresponding author} ; ^{fengzhangchem@yahoo.com" class="auth_mail" title="E-mail the corresponding author}
关键词：Sulfonamides ; Ultra-high performance supercritical fluid chromatography (UHPSFC) ; PDA ; Serum ; Resolution
刊名：Journal of Chromatography A
出版年：2016
出版时间：5 February 2016
年：2016
卷：1432
期：Complete
页码：132-139
全文大小：1331 K

文摘

•: Near baseline separation for 15 sulfonamides and metabolites by UHPSFC was achieved.
•: Stationary phases, modifiers, additives, column temperature, ABPR backpressure and flow rate were optimized for baseline separate 15 sulfonamides.
•: UHPSFC-PDA for determination 15 sulfonamides and metabolites in serum.
•: Simple, accurate, green, low cost, faster separations and better resolution.
•: Assumed that the retention behavior of sulfonamides on BEH column may mainly depend on the molecule polarity.