Amphetamine and derivatives in natural weight loss pills and dietary supplements by capillary electrophoresis-tandem mass spectrometry

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Amphetamine and derivatives in natural weight loss pills and dietary supplements by capillary electrophoresis-tandem mass spectrometry

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作者：Vagner Bezerra dos Santos^a ; ^{vagnerbs@ufpa.br" class="auth_mail" title="E-mail the corresponding author} ; Daniela Daniel^b ; ^{daniel@agilent.com" class="auth_mail" title="E-mail the corresponding author} ; Melina Singh^c ; ^{MSINGH13@ubishops.ca" class="auth_mail" title="E-mail the corresponding author} ; Prof. Dr. Claudimir Lucio do Lago^a ; ^{claudemi@iq.usp.br" class="auth_mail" title="E-mail the corresponding author}
关键词：Amphetamine (PubChem CID 3007) ; β-methylphenylethylamine (PubChem CID 11398) ; Phentermine (PubChem CID 4771) ; Methamphetamine (PubChem CID 10836) ; Methylenedioxyamphetamine (PubChem CID 297310) ; Methylenedioxymethamphetamine (PubChem CID 1615) ; Methylenedioxyethylamphetamine (PubChem CID 3057998)
刊名：Journal of Chromatography B, Analytical Technologies in the Biomedical and Life Sciences
出版年：2016
出版时间：1 December 2016
年：2016
卷：1038
期：Complete
页码：19-25
全文大小：969 K

文摘

•: A CE-MS approach for amphetamines in weight loss pills is introduced.
•: A modified QuEChERS (at high pH) allowed for a simple and efficient cleanup step.
•: Recoveries ranging from 85 to 123% were obtained.
•: Limits of Detection were lower than 0.06 μg L⁻¹.

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