Koenigs-Knorr reaction of fusel alcohols with methyl (1-bromo-2,3,4-tri-O-acetyl-¦Á-d-glucopyranosid)uronate leading to the protected alkyl glucuronides¡ªcrystal structures and high resolution ¹H and ¹³C NMR data

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• 作者：Bettina Mö ; nch ; Antje Gebert ; Franziska Emmerling ; Roland Becker ; ^{roland.becker@bam.de} ; Irene Nehls
• 关键词：d-Glucuronic acid derivates ; X-ray analysis ; High resolution NMR ; Anomeric configuration ; Synthesis
• 刊名：Carbohydrate Research
• 出版年：2012
• 出版时间：1 May, 2012
• 年：2012
• 卷：352
• 期：Complete
• 页码：186-190
• 全文大小：274 K

文摘

Crystal structures and high resolution ¹H and ¹³C NMR spectral data for methyl (alkyl 2,3,4-tri-O-acetyl-¦Â-d-glucopyranosid)uronates (alkyl = methyl, ethyl, n-propyl, i-propyl, n-butyl, sec-butyl, i-butyl, n-pentyl, 2-methyl-1-butyl and 3-methyl-1-butyl) are presented.