Antisolvent crystallization of aqueous ammonium dihydrogen phosphate solutions by addition of methanol

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Antisolvent crystallization of aqueous ammonium dihydrogen phosphate solutions by addition of methanol

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作者：Keshra Sangwal^a ; Ewa Mielniczek-Brzó ; ska^b ; ^{e.mielniczek@ajd.czest.pl" class="auth_mail" title="E-mail the corresponding author}
关键词：A1. Antisolvent crystallization ; A1. Metastable zone width ; A1. Kinetics ; B1. Ammonium dihydrogen phosphate
刊名：Journal of Crystal Growth
出版年：2016
出版时间：1 October 2016
年：2016
卷：451
期：Complete
页码：139-149
全文大小：2287 K

文摘

•: Crystallization of ADP from aqueous solutions is studied by feeding antisolvent methanol.
•: In situ transmitted laser beam intensity and solution temperature measurements are used.
•: Sensitivity of the two methods for three-dimensional (3D) nucleation is compared.
•: Solution temperature measurements are more reliable for detection of 3D nucleation.
•: Processes involved during antisolvent crystallization are analyzed and discussed.

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