Optimization of a rapid QuEChERS sample treatment method for HILIC-MS<sup>2</sup> analysis of paralytic shellfish poisoning (PSP) toxins in mussels

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Optimization of a rapid QuEChERS sample treatment method for HILIC-MS² analysis of paralytic shellfish poisoning (PSP) toxins in mussels

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作者：Monica Mattarozzi^a ; ^{monica.mattarozzi@unipr.it" class="auth_mail" title="E-mail the corresponding author} ; Marco Milioli^a ; Federica Bianchi^a ; Antonella Cavazza^a ; Silvia Pigozzi^b ; Anna Milandri^b ; Maria Careri^a
关键词：Paralytic shellfish poisoning (PSP) toxins ; Hydrophilic interaction liquid chromatography-tandem mass spectrometry (HILIC-MS2) ; Mussels ; QuEChERS ; Experimental design optimization
刊名：Food Control
出版年：2016
出版时间：February 2016
年：2016
卷：60
期：Complete
页码：138-145
全文大小：1130 K

文摘

•: Development of a rapid sample pretreatment for saxitoxins determination in mussels.
•: QuEChERS protocol optimisation by multivariate approach.
•: Analytical method by HILIC-ESI-MS² successfully validated.
•: Suitability of the method for analysis of samples from different areas.

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