Enhanced efficiency of solid-state NMR investigations of energy materials using an external automatic tuning/matching (eATM) robot

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• 作者：Oliver Pecher^a ; ¹ ; David M. Halat^a ; ¹ ; Jeongjae Lee^a ; Zigeng Liu^a ; Kent J. Griffith^a ; Marco Braun^b ; Clare P. Grey^a ; ^{cpg27@cam.ac.uk}
• 关键词：Automation ; VOCS ; Spin-echo-mapping ; Ex situ NMR ; Li-/Na-ion battery ; Energy storage materials
• 刊名：Journal of Magnetic Resonance
• 出版年：2017
• 出版时间：February 2017
• 年：2017
• 卷：275
• 期：Complete
• 页码：127-136
• 全文大小：1447 K
• 卷排序：275

文摘

New external automatic tuning/matching (eATM) robot system. Enables “on-the-fly” recalibration of the resonance circuit during NMR experiments. Enhanced efficiency of variable offset cumulative spectra (VOCS) and other broadband measurements. Various applications to paramagnetic, quadrupolar, and/or multinuclear systems. Automated acquisition during variable temperature, static, and/or MAS NMR experiments.