A practical ortho-rearrangement of silyl group of ortho-bromophenyl silyl ethers using magnesium(0)

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A practical ortho-rearrangement of silyl group of ortho-bromophenyl silyl ethers using magnesium(0)

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作者：Takashi Hasegawa^a ; ^b ; Hisanori Kishida^b ; Nobuyoshi Nomura^a ; ^{nnomura@nagoya-u.jp}
关键词：Grignard reagent ; Magnesium ; retro-Brook rearrangement ; ortho-Silylphenol ; Salen
刊名：Tetrahedron Letters
出版年：2017
出版时间：1 February 2017
年：2017
卷：58
期：5
页码：455-457
全文大小：648 K
卷排序：58

文摘

Synthesis of ortho-silylphenol from ortho-bromophenyl silyl ether using Mg(0). retro-Brook rearrangement by Grignard reagents. Large scale synthesis of ortho-silylphenol.