Liquid chromatography mass spectrometry determination of perfluoroalkyl acids in environmental solid extracts after phospholipid removal and on-line turbulent flow chromatography purification

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Liquid chromatography mass spectrometry determination of perfluoroalkyl acids in environmental solid extracts after phospholipid removal and on-line turbulent flow chromatography purification

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作者：M. Mazzoni ; S. Polesello ; M. Rusconi ; S. Valsecchi ; ^{valsecchi@irsa.cnr.it" class="auth_mail" title="E-mail the corresponding author}
关键词：Turbulent flow chromatography ; PFOA ; PFOS ; Perfluorinated compounds ; Phospholipid removal ; Environmental solid matrices
刊名：Journal of Chromatography A
出版年：2016
出版时间：1 July 2016
年：2016
卷：1453
期：Complete
页码：62-70
全文大小：1222 K

文摘

•: TFC is useful for the on-line clean-up of extracts of solid matrices.
•: On-line TFC was able to remove most of phospholipids in biological extracts.
•: Phospholipids in the extracts were totally removed by HybridSPE^® cartridges.
•: An on-line TFC/UHPLC–MS/MS method was developed for PFAA analysis in solid samples.
•: The method was applied to the analysis of mussels, clams, fish, eggs and sediments.

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