Sampling methods were evaluated for determination of fumarolic sulfur species.
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Fixation of H2S as Ag2S(s), unsuitable for HCl detection, underrates H2S and SO2.
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Fixation of H2S as S(0) overestimates SO2, but this phase is stable against O2.
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Fixation of H2S as CdS(s) gives agreeable results, but CdS(s) is readily oxidized.
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