Growth Kinetics of the Fe2B Coating on AISI H13 Steel

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• 作者：M. Keddam ; M. Ortiz-Domínguez…
• 关键词：Boriding ; Iron boride ; Incubation time ; Kinetic model ; Activation energy
• 刊名：Transactions of the Indian Institute of Metals
• 出版年：2015
• 出版时间：June 2015
• 年：2015
• 卷：68
• 期：3
• 页码：433-442
• 全文大小：1,731 KB
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• 作者单位：M. Keddam (1)
  M. Ortiz-Domínguez (2)
  M. Elias-Espinosa (3)
  O. Damián-Mejía (4)
  A. Arenas-Flores (5)
  O. A. Gómez-Vargas (6)
  M. Abreu-Quijano (2)
  Jorge Iván Aldana-González (7)
  J. Zuno-Silva (2)
  
  1. Laboratoire de Technologie des Matériaux, Faculté de Génie Mécanique et Génie des Procédés, USTHB, B.P. No. 32, El-Alia, Bab-Ezzouar, 16111, Algiers, Algeria
  2. Escuela Superior Cd. Sahagún, Universidad Autónoma del Estado de Hidalgo, UAEH, Carretera Cd. Sahagún-Otumba s/n, 43990, Pachuca, Hidalgo, Mexico
  3. Instituto Tecnológico y de Estudios Superiores de Monterrey-ITESM Campus Santa Fe, Av. Carlos Lazo No. 100, Del. álvaro Obregón, CP 01389, Mexico, D.F., Mexico
  4. Instituto de Investigación en Materiales, Universidad Nacional Autónoma de México-UNAM, Circuito Exterior, s/n Ciudad Universitaria, CP 04510, Coyoacán, D.F., Mexico
  5. Centro de Investigación en Materiales y Metalurgia, Universidad Autónoma del Estado de Hidalgo, Ciudad Universitaria Pachuca-Tulancingo km. 4.5, Pachuca, Hidalgo, Mexico
  6. Instituto Tecnológico de Tlalnepantla-ITTLA, Av. Instituto Tecnológico, S/N. Col. La Comunidad, CP 54070, Tlalnepantla de Baz, Estado de México, Mexico
  7. Universidad Tecnológica de México, Blvd. Calacoaya No. 7, Col. La Ermita, 52970, Atizapán de Zaragoza, Estado de México, Mexico
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Materials Science
  Metallic Materials
  Materials Science, general
  Tribology, Corrosion and Coatings
  
• 出版者：Springer India
• ISSN：0975-1645

文摘

A kinetic model was suggested to study the growth kinetics of Fe₂B layers on AISI H13 steel via the pack-boriding method in the temperature range of 1,123-,273?K. This model was based of the principle of mass conservation at the (Fe₂B/substrate) interface where the boride incubation time was independent of the boriding temperature. The model was also validated experimentally by comparing the experimental Fe₂B layers thicknesses with the predicted values at 1,173?K during 7?h, 1,223?K during 5?h, 1,253?K during 2?h and 1,273?K for 3?h. The Fe₂B layers grown on AISI H13 steel were characterized by use of the following experimental techniques: optical microscopy, scanning electron microscopy, energy dispersive X-ray spectroscopy and X-ray diffraction analysis. In addition, a contour diagram describing the evolution of Fe₂B layers as a function of the boriding parameters (time and temperature) was proposed. Finally, the boron activation energy for AISI H13 steel was estimated as 233?kJ?mol? on the basis of our experimental results. This value of energy was compared with the literature data.