Carbon nanotube-ionic liquid nanocomposite modified carbon-ceramic electrode for determination of dopamine in real samples

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• 作者：Mir Reza Majidi (1251)
  Reza Fadakar Bajeh Baj (1251)
  Abdolhossein Naseri (1251)
  
• 关键词：Multi walled carbon nanotubes ; Ionic liquid ; Nanocomposite ; Dopamine ; Carbon ; ceramic electrode
• 刊名：Central European Journal of Chemistry
• 出版年：2013
• 出版时间：July 2013
• 年：2013
• 卷：11
• 期：7
• 页码：1172-1186
• 全文大小：2934KB
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• 作者单位：Mir Reza Majidi (1251)
  Reza Fadakar Bajeh Baj (1251)
  Abdolhossein Naseri (1251)
  
  1251. Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, 51664, Iran
  
• ISSN：1644-3624

文摘

Room temperature 1-butyl-3-methylimidazolium tetraflouroborate ([BMIM][BF4]) ionic liquid was employed for dispersion of multi walled carbon nanotubes (MWCNTs) and the formation of nanocomposite on the surface of a carbon-ceramic electrode. The surface of the modified electrode was characterized using scanning electron microscopy and electrochemical impedance spectroscopy. The modified electrode exhibited excellent electrochemical activity to oxidation of dopamine (DA); whereas electro oxidation of ascorbic acid (AA) was not seen and electro oxidation of uric acid (UA) appeared at a more positive potential than DA. The multi walled carbon nanotube-ionic liquid nanocomposite modified carbon-ceramic electrode was used for the selective determination of DA in the presence of high levels of AA and UA using differential pulse voltammetry. The calibration curve for DA was linear in the range of 3.00 to 130 μM with the detection limit (S/N=3) of 0.87 μM. The present electrode was successfully applied to the determination of DA in some commercial pharmaceutical samples and human blood serum.