A heteropolyacid-based ionic liquid immobilized onto Fe3O4/SiO2/Salen/Mn as an environmentally friendly catalyst for synthesis of cyclic carbonate

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• 作者：Seyed Mohsen Sadeghzadeh
• 关键词：Magnetic nanoparticles (MNPs) ; Salen ; Green Chemistry ; Ionic liquid ; Heteropolyacid ; Cyclic carbonate
• 刊名：Research on Chemical Intermediates
• 出版年：2016
• 出版时间：March 2016
• 年：2016
• 卷：42
• 期：3
• 页码：2317-2328
• 全文大小：656 KB
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• 作者单位：Seyed Mohsen Sadeghzadeh (1)
  
  1. Department of Chemistry, Sina Masihabadi Student Research, P.O. Box 97175-615, Neishabour, Iran
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Catalysis
  Physical Chemistry
  Inorganic Chemistry
  
• 出版者：Springer Netherlands
• ISSN：1568-5675

文摘

Magnetite-polyoxometalate hybrid nanomaterials, Fe₃O₄/SiO₂/Salen/Mn/IL/HPW (MNPs-HPW), was prepared by grafting of H₃PW₁₂O₄₀ on the ionic liquid-functionalized Fe₃O₄ magnetite nanoparticles. This catalyst is a recoverable catalyst for the one-pot synthesis of cyclic carbonate derivatives in high to excellent yield under solvent-free conditions. The MNPs-HPW catalyst was characterized via Fourier transform infrared spectroscopy, X-ray diffraction, thermal gravimetric analysis, transmission electron microscopy, and a vibrating sample magnetometer. Moreover, the catalyst could be easily recovered by magnetic separation and recycled for ten times without significant loss of its catalytic activity.