A self-stiffness finishing for cotton fabric with N-methylmorpholine-N-oxide

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• 作者：Fang Xu ; Yulian Yang ; Guangxian Zhang ; Fengxiu Zhang ; Yuansong Zhang
• 关键词：Cotton fabric ; N ; methylmorpholine ; N ; oxide ; Self ; stiffness ; No auxiliaries
• 刊名：Cellulose
• 出版年：2015
• 出版时间：August 2015
• 年：2015
• 卷：22
• 期：4
• 页码：2837-2844
• 全文大小：1,016 KB
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• 作者单位：Fang Xu (1) (3)
  Yulian Yang (1) (3)
  Guangxian Zhang (1) (3)
  Fengxiu Zhang (2)
  Yuansong Zhang (1) (3)
  
  1. College of Textiles and Garments, Southwest University, Chongqing, 400715, China
  3. Chongqing Engineering Research Center of Biomaterial Fiber and Modern Textile, Chongqing, 400715, China
  2. College of Chemistry and Chemical Engineering, Southwest University, Chongqing, 400715, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Bioorganic Chemistry
  Physical Chemistry
  Organic Chemistry
  Polymer Sciences
  
• 出版者：Springer Netherlands
• ISSN：1572-882X

文摘

In this study, the surface layer of cotton fabric was swelled with N-methylmorpholine-N-oxide with 18?% water content, washed and dried to improve its stiffness property. Finally, the finished fabric had no auxiliaries and self-stiffened. The results showed that the bending rigidity increased from 0.75?×?105 to 1.57?×?105?mN?cm, the acute elastic crease recovery angle from 95.2° to 117.3°, the delayed elastic crease recovery angle from 117.6° to 146.6° and the moisture regain from 8.07 to 10.3?%. The stiffness was almost unaffected by 30 multiple washing times. The tear strength, breaking strength and whiteness properties remained excellent. Scanning electron microscopy showed that the edges of finished fibres obviously curled. According to infrared spectrum analysis, no new groups were found. X-ray diffraction analysis showed that the crystal structure of the fibre changed, with cellulose?II formed disorderly in the surface layer of the cotton fibres. This mechanism permits the cotton fabric to self-stiffen in the modifying process.