Synthesis and physical–chemical properties of N-containing nanoporous carbons

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• 作者：Nataliya D. Shcherban (1)
  Svitlana M. Filonenko (1)
  Pavel S. Yaremov (1)
  Vyacheslav S. Dyadyun (1)
  
• 刊名：Journal of Materials Science
• 出版年：2014
• 出版时间：June 2014
• 年：2014
• 卷：49
• 期：12
• 页码：4354-4362
• 全文大小：990 KB
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• 作者单位：Nataliya D. Shcherban (1)
  Svitlana M. Filonenko (1)
  Pavel S. Yaremov (1)
  Vyacheslav S. Dyadyun (1)
  
  1. L.V. Pisarzhevsky Institute of Physical Chemistry, NAS of Ukraine, 31 pr. Nauky, Kyiv, 03028, Ukraine
  
• ISSN：1573-4803

文摘

Meso- and microporous nitrogen-containing carbons, characterized by homogeneous meso- (V?=?1.00?cm3/g, D?=?3.5?nm) and microporous (V up to 0.26?cm3/g, D?≈?.5?nm) structure, and the presence of basic groups (up to 1.7?mmol/g) were obtained by matrix and bulk carbonization of sucrose in the presence of melamine or urea. It is shown that obtained N-containing microporous carbons possess good interfacial capacitance (0.21?F/m2) and they are characterized with stability during repeated charge–discharge cycles. Synthesized N-containing nanoporous carbons show higher adsorption of carbon dioxide (up to 6.3?mmol/g at ?0?°C) than the samples without nitrogen (up to 3.9?mmol/g at ?0?°C).