Characterization of high-alumina coal fly ash based silicate material and its adsorption performance to CO2

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• 作者：Yinan Yan ; Yajun Gao ; Wenjing Tang ; Qiang Li…
• 关键词：Silicate Material ; High ; alumina Coal Fly Ash (HACFA) ; Carbon Dioxide (CO2) ; Adsorption ; Regeneration
• 刊名：Korean Journal of Chemical Engineering
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：33
• 期：4
• 页码：1369-1379
• 全文大小：1,276 KB
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• 作者单位：Yinan Yan (1)
  Yajun Gao (1)
  Wenjing Tang (1)
  Qiang Li (1)
  Jianbin Zhang (1)
  
  1. College of Chemical Engineering, Inner Mongolia University of Technology, Huhhot, 010051, China
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Industrial Chemistry and Chemical Engineering
  Catalysis
  Materials Science
  Biotechnology
  
• 出版者：Springer New York
• ISSN：1975-7220

文摘

Silicate material prepared from high-alumina coal fly ash (HACFA) was characterized by using XRD, SEM, FTIR spectroscopy, TGA-DSC, and elemental analysis. These spectral results show that the silicate material is mainly composed of eight elements—O, C, Si, Ca, Na, Mg, Al, and Fe, which exist as the formations of Ca2+, Na+, Mg2+, Al3+, Fe3+, SiO ₃ 2− , and COO ₃ 2− , and some adsorbed water and crystal water are determined in the silicate material. The material with surface area of 117.12m2/g shows a faveolate structure, and a pore size distribution of silicate material is calculated at 11.01 nm from the nitrogen desorption isotherm using the BJH model. When the material was used for CO₂ adsorption at T=323.15 K and flow rate=95mL/min with 15.79% (vol) CO₂, a dynamic adsorption capacity of CO₂ on the surface of silicate material was found at 8.67mg/g and the adsorption values decreased weakly after seventeen recycling times. The investigation of dynamic adsorption behavior shows that the silicate material presents similar adsorption properties with commercial active carbon and stronger adsorption properties than commercial diatomite.