Grain boundary segregation in Al–Mn electrodeposits prepared from ionic liquid

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Grain boundary segregation in Al–Mn electrodeposits prepared from ionic liquid

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作者：Ting-Yun Huang ; Christopher J. Marvel ; Patrick R. Cantwell…
刊名：Journal of Materials Science
出版年：2016
出版时间：January 2016
年：2016
卷：51
期：1
页码：438-448
全文大小：3,151 KB
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作者单位：Ting-Yun Huang (1)
Christopher J. Marvel (2)
Patrick R. Cantwell (3)
Martin P. Harmer (2)
Christopher A. Schuh (1)

1. Departments of Materials Science and Engineering, Massachusetts Institute of Technology, 77 Massachusetts Avenue, Cambridge, MA, 02139, USA
2. Department of Materials Science and Engineering, Lehigh University, 27 Memorial Dr W, Bethlehem, PA, 18015, USA
3. Department of Mechanical Engineering, Rose-Hulman Institute of Technology, 5500 Wabash Ave, Terre Haute, IN, 47803, USA
刊物类别：Chemistry and Materials Science
刊物主题：Chemistry
Materials Science
Characterization and Evaluation Materials
Polymer Sciences
Continuum Mechanics and Mechanics of Materials
Crystallography
Mechanics
出版者：Springer Netherlands
ISSN：1573-4803

文摘

Among the various preparation methods for nanocrystalline alloys, ionic liquid electrodeposition at low temperature is of interest for its scalability and efficiency. To achieve nanostructures with stabilized structures, it is desirable to directly deposit alloys in which the grain boundaries are decorated with a segregated alloying element. Here a combination of atom-probe tomography and aberration-corrected scanning transmission electron microscopy are used to confirm that in Al–Mn nanocrystalline alloys deposited from an ionic liquid, Mn is slightly segregated at grain boundaries in the as-deposited condition. The apparent heat of grain boundary segregation is calculated to lie between 1100 and 1500 J mol−1, which aligns reasonably well with a value calculated using a Miedema-based segregation model, and which is also in line with a more refined CALPHAD-type estimation if it is assumed that the Al–Mn deposits are not fully equilibrated at the deposition temperature.