Synthesis and Characterization of Bi1.6Pb0.4Sr2Ca2Cu3O7 Superconducting Oxide by High-Energy Milling

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• 作者：Nono Darsono ; Agung Imaduddin ; Kati Raju…
• 关键词：High ; energy milling ; Superconductor ; Bi ; Pb ; Sr ; Ca ; Cu oxide ; XRD ; SEM
• 刊名：Journal of Superconductivity Incorporating Novel Magnetism
• 出版年：2015
• 出版时间：August 2015
• 年：2015
• 卷：28
• 期：8
• 页码：2259-2266
• 全文大小：2,264 KB
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• 作者单位：Nono Darsono (1) (2)
  Agung Imaduddin (2)
  Kati Raju (1)
  Dang-Hyok Yoon (1)
  
  1. School of Materials Science and Engineering, Yeungnam University, Gyeongsan, 712-749, South Korea
  2. Research Center for Metallurgy of Materials, Indonesian Institute of Sciences, Gd. 470, Kawasan Puspiptek, Serpong, Tangerang Selatan, 15314, Indonesia
  
• 刊物类别：Physics and Astronomy
• 刊物主题：Physics
  Superconductivity, Superfluidity and Quantum Fluids
  Magnetism and Magnetic Materials
  Condensed Matter
  Characterization and Evaluation Materials
  
• 出版者：Springer New York
• ISSN：1557-1947

文摘

Superconducting Bi1.6Pb0.4Sr2Ca2Cu3O7 was prepared by a solid-state reaction using high-energy milling for the starting materials. The effects of the sintering temperature and time on the phase evolution, microstructure, and superconducting properties were examined by thermogravimetric analysis, X-ray diffraction, scanning electron microscopy, and four-point probe resistivity measurements. High-energy milling decreased the precursor particle size to approximately 30 nm with a relatively uniform distribution of multi-compositions. Because of the mechanochemical activation for the starting materials, the reaction temperature was decreased to 750 ?/sup>C due to the decreased diffusion length required for the solid-state reaction. Bi1.6Pb0.4Sr2Ca2Cu3O7 prepared by high-energy milling showed good superconducting properties with T c?100 K, which is superior to the same material prepared by ball milling and sol-gel routes.