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Removal of uranium anionic species from aqueous solutions by polyethylenimine–epichlorohydrin resins
- 作者:S. Sarri (1)
P. Misaelides (1) D. Zamboulis (1) L. Papadopoulou (2) J. Warcho? (3)
- 关键词:Sorption ; Polyethylenimine–epichlorohydrin resin ; Uranyl ; carbonato anions ; Uptake kinetics
- 刊名:Journal of Radioanalytical and Nuclear Chemistry
- 出版年:2013
- 出版时间:March 2013
- 年:2013
- 卷:295
- 期:3
- 页码:1731-1736
- 全文大小:468KB
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- 作者单位:S. Sarri (1)
P. Misaelides (1) D. Zamboulis (1) L. Papadopoulou (2) J. Warcho? (3)
1. Department of Chemistry, Aristotle University, 54124, Thessaloniki, Greece 2. Department of Physics, Aristotle University, 54124, Thessaloniki, Greece 3. Department of Water Purification and Protection, Rzeszow University of Technology, Rzeszow, Poland
- ISSN:1588-2780
文摘
The removal of uranium anionic species from aqueous solutions (initial concentration: 10-,000?mg/L) by a low- and a high molecular weight polyethylenimine–epichlorohydrin resins was studied in the absence of background electrolytes at initial pH (pHinit) 8 to10. The amount of the sorbed U was determined spectrophotometrically using the Arsenazo III method. The maximum uptake was observed at pHinit 8 using both resins. The maximum uptake capacity observed was 221 and 388?mg U/g for the low- and high molecular weight resin respectively. The uptake data were modeled using a number of 2- and 3- parametric isotherm equations (Langmuir, Freundlich, Langmuir–Freundlich, Toth and Redlich–Peterson). The kinetics of the uranium removal was also studied and modeled using the pseudo-first and pseudo-second order equations. The surface and interior of the resin grains were examined after the sorption experiments by scanning electron microscopy/energy dispersive spectroscopy.
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