Simultaneous Voltammetric Determination of Synthetic Colorants in Foods Using a Magnetic Core–Shell Fe3O4@SiO2/MWCNTs Nanocomposite Modified Carbon Paste Elect

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• 作者：Majid Arvand ; Yasaman Parhizi ; Seyed Hadi Mirfathi
• 关键词：Magnetic nanocomposite ; Core–shell Fe3O4@SiO2 nanoparticles ; Multi ; walled carbon nanotube ; Sunset yellow ; Tartrazine ; Square wave voltammetry
• 刊名：Food Analytical Methods
• 出版年：2016
• 出版时间：April 2016
• 年：2016
• 卷：9
• 期：4
• 页码：863-875
• 全文大小：2,103 KB
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• 作者单位：Majid Arvand (1)
  Yasaman Parhizi (1)
  Seyed Hadi Mirfathi (1)
  
  1. Electroanalytical Chemistry Laboratory, Faculty of Science, University of Guilan, Namjoo Street, P.O. Box 1914-41335, Rasht, Iran
  
• 刊物类别：Chemistry and Materials Science
• 刊物主题：Chemistry
  Food Science
  Chemistry
  Microbiology
  Analytical Chemistry
  
• 出版者：Springer New York
• ISSN：1936-976X

文摘

This paper reports the production of a novel magnetic nanocomposite based on multi-walled carbon nanotubes (MWCNTs) decorated with magnetic core–shell Fe₃O₄@SiO₂ nanoparticles which were used to fabricate a modified carbon paste electrode (Fe₃O₄@SiO₂/MWCNT-CPE). The Fe₃O₄@SiO₂/MWCNT-CPE was investigated for the simultaneous determination of sunset yellow (SY) and tartrazine (TT) in 0.1 mol/L phosphate buffer solution (pH 6.0) using square wave voltammetry (SWV). The synthesized nanocomposite was characterized by transmission electron microscopy, scanning electron microscopy, energy dispersive spectroscopy and Fourier transform infrared spectroscopy. The proposed electrode exhibits linear ranges of 0.5–100 μmol/L SY and TT with detection limits of 0.05 and 0.04 μmol/L for SY and TT, respectively. The novel proposed voltammetric method was successfully applied in the simultaneous determination of SY and TT in food products, with results similar to those obtained using a HPLC method at 95 % confidence level.