测定油脂极性组分不同柱层析技术的比较
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  • 英文篇名:Comparison of different column chromatography detection methods on polar compounds in oils and fats
  • 作者:薛斌 ; 姜元荣 ; 曹文明 ; 王俊杰
  • 英文作者:XUE Bin;JIANG Yuanrong;CAO Wenming;WANG Junjie;Wilmar (Shanghai ) Biotechnology Research & Development Center Co.,Ltd.;Shanghai Grain Science Research Institute;
  • 关键词:制备型快速柱层析 ; 柱层析 ; 极性组分 ; 油脂 ; 煎炸油 ; 餐厨废油脂
  • 英文关键词:preparative flash column chromatography;;column chromatography;;polar component;;oils and fats;;frying oil;;waste cooking oil
  • 中文刊名:ZYZZ
  • 英文刊名:China Oils and Fats
  • 机构:丰益(上海)生物技术研发中心有限公司;上海市粮食科学研究所;
  • 出版日期:2018-03-15 10:51
  • 出版单位:中国油脂
  • 年:2018
  • 期:v.43;No.324
  • 语种:中文;
  • 页:ZYZZ201802031
  • 页数:4
  • CN:02
  • ISSN:61-1099/TS
  • 分类号:148-151
摘要
以现行的油脂极性组分检测ISO 8420(2002)为依据,对GB/T 5009.202—2003《食用植物油煎炸过程中的极性组分(PC)的测定》的柱层析法,GB 5009.202—2016《食品安全国家标准食用油中极性组分(PC)的测定》中的制备型快速柱层析法和柱层析法进行比对实验。结果发现:GB/T 5009.202—2003的柱层析法的检测结果与ISO标准的检测结果差异较大,一致性差;而GB 5009.202—2016中的制备型快速柱层析法和柱层析法的检测结果与ISO标准的检测结果基本一致。
        According to the column chromatography method in ISO 8420( 2002),the results of polar compounds content detected according to the column chromatography method in GB/T 5009. 202—2003 Determination of Polar Compounds in Edible Vegetable Oils Used in Frying Food and the preparative flash column chromatography method & the column chromatography method in GB 5009. 202—2016 National Food Safety Standards Determination of Polar Compounds in Edible Oils were compared. The results showed that the results acquired by the column chromatography method in GB/T 5009. 202—2003 had obvious differences with those acquired by the column chromatography method in ISO 8420( 2002). But the results acquired by the preparative flash column chromatography method & the column chromatography method in GB 5009.202—2016 were in accordance with those acquired by the column chromatography method in ISO 8420( 2002).
引文
[1]印瑜洁,薛斌.硅胶柱层析分离煎炸油中极性和非极性组分的研究[J].粮食与油脂,2016,29(6):72-74.
    [2]曹文明,薛斌,陈凤香,等.三酰甘油氧化聚合物的制备型快速柱层析-体积排阻色谱测定方法[J].分析测试学报,2012,31(8):933-939.
    [3]CAO W M,ZHANG K Y,XUE B,et al.Determination of oxidized triacylglycerol polymers by preparative flash chromatography and high-performance size-exclusion chromatography[J].Asian J Chem,2013,25(16):9189-9149.
    [4]FEREIDOON S.贝雷油脂化学与工艺学:第一卷[M].王兴国,金青哲,译.6版.北京:中国轻工业出版社,2016:352.
    [5]中华人民共和国卫生部,中国国家标准化管理委员会.食用植物油煎炸过程中的卫生标准:GB 7102.1—2003[S].北京:中国标准出版社,2003:1.
    [6]International Standard Organization.Animal and vegetable fats and oils-Determination of content of polar compounds:ISO 8420(2002)[S].Switzerland:ISO Press,2002:1-8.
    [7]American Oil Chemists’Society.Determination of polar compounds in frying fats:AOCS.Official Method Cd20-91[S].USA:AOCS Press,2009:1-6.
    [8]Association of Official Analytical Chemists.Polar components in frying fats chromatographic method:AOAC Official Method 982.27[S].USA:AOAC Press,2012:31-32.
    [9]International Union of Pure and Applied Chemistry.Determination of polar compounds in frying fats:IUPAC 2.507[S].7th ed.Oxford:Blackwell,1992:216-219.
    [10]中华人民共和国卫生部,中国国家标准化管理委员会.食用植物油煎炸过程中的极性组分(PC)的测定:GB/T 5009.202—2003[S].北京:中国标准出版社,2003:1-3.
    [11]中华人民共和国卫生与计划生育委员会.食品安全国家标准食用油中极性组分(PC)的测定:GB 5009.202—2016[S].北京:中国标准出版社,2016:1-10.
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