电感耦合等离子体质谱测定硫的方法研究及应用进展

详细信息    查看全文 | 推荐本文 |

英文篇名：Advances and Applications in Method for Determination of Sulfur by Inductively Coupled Plasma Mass Spectrometry 作者：黄志丁 ; 王军 ; 逯海 ; 杨晓进 英文作者：HUANG Zhi-ding1,WANG Jun2,LU Hai2,YANG Xiao-jin1(1.College of Chemical Engineering,Beijing University of Chemical Technology,Beijing 100029,China; 2.National Institute of Metrology,Beijing 100013,China) 关键词：电感耦合等离子体质谱(ICP-MS) ; 硫 ; 进展 英文关键词：inductively coupled plasma mass spectrometry(ICP-MS);sulfur;progress 中文刊名：ZPXB 英文刊名：Journal of Chinese Mass Spectrometry Society 机构：北京化工大学化学工程学院;中国计量科学研究院; 出版日期：2013-01-15 出版单位：质谱学报 年：2013 期：v.34 基金：2009年度质检公益性行业科研专项(200910105)资助 语种：中文; 页：ZPXB201301009 页数：8 CN：01 ISSN：11-2979/TH 分类号：59-66

摘要

硫是矿石、化石燃料、蛋白质等的重要组成元素,与人类生活密切相关。近年来,随着质谱技术的发展,电感耦合等离子体质谱(ICP-MS)已成为硫测量和研究的重要手段,并在环境监测、食品安全、生命科学、环境地球化学等研究中显示出良好的应用前景。本工作综述了ICP-MS用于硫元素总量、多种形态、硫同位素测量技术方面的最新研究进展。
        Sulfur is constituent element of ores,fossil fuels and proteins,it plays a great role in human life.Recently,with the development of mass spectrometry,inductively coupled plasma mass spectrometry(ICP-MS) has become an important technology for measurement and study of sulfur,and it has the broad application prospect in fields of environmental science,food safety,life science and geochemical.The progresses in the measurement of sulfur content,sulfur species and sulfur isotopes by ICP-MS were reviewed in this paper.

引文

[1]GILL B C,LYONS T W,YOUNG S A,et al.Geochemical evidence for widespread euxinia in the Later Cambrian ocean[J].Nature,2011,469(7328):80-83.
    [2]WIND M,WEGENER A,EISENMENGER A,et al.Sulfur as the key element for quantitative protein analysis by capillary liquid chromatogra-phy coupled to element mass spectrometry[J].Angewandte Chemie International Edition,2003,42(29):3425-3427.
    [3]CARROLL M R.Climate change:Volcanic sul-phur in the balance[J].Nature,1997,389(6651):543-544.
    [4]BURAKHAM R,HIGUCHI K,OSHIMA M,et al.Flow injection spectrophotometry coupled with a crushed barium sulfate reactor column for the de-termination of sulfate ion in water samples[J].Talanta,2004,64(5):1147-1150.
    [5]OHIRA S I,TODA K.Ion chromatographic meas-urement of sulfide,methanethiolate,sulfite and sulfate in aqueous and air samples[J].J Chroma-togr A,2006,1121(2):280-284.
    [6]中国石油大庆油田工程有限公司分析检测中心.GB/T17606—2009原油中硫含量的测定[S].北京:中国标准出版社,2009.
    [7]HOUK R S,FASSEL V A,FLESCH G D,et al.Inductively coupled argon plasma as an ion source for mass spectrometric determination of trace ele-ments[J].Anal Chem,1980,52(14):2283-2289.
    [8]AMMANN A A.Inductively coupled plasma mass spectrometry(ICP MS):A versatile tool[J].J Mass Spectrom,2007,42(4):419-427.
    [9]BEAUCHEMIN D.Inductively coupled plasma mass spectrometry[J].Anal Chem,2008,80(12):4455-4486.
    [10]MASON P R D,KASPERS K,BERGEN M J.Determination of sulfur isotope ratios and concen-trations in water samples using ICP-MS incorpo-rating hexapole ion optics[J].J Anal Atom Spec-trom,1999,14(7):1067-1074.
    [11]BANDURA D R,BARANOV V I,TANNER S D.Detection of ultratrace phosphorus and sulfur by quadrupole ICPMS with dynamic reaction cell[J].Anal Chem,2002,74(7):1497-1502.
    [12]WOLF K D,BALCAEN L,Van De WALLE E,et al.A comparison between HPLC-dynamic re-action cell-ICP-MS and HPLC-sector field-ICP-MS for the detection of glutathione-trapped reac-tive drug metabolites using clozapine as a model compound[J].J Anal Atom Spectrom,2010,25(3):419-425.
    [13]PROHASKA T,LATKOCZY C,STINGEDER G.Precise sulfur isotope ratio measurements in trace concentration of sulfur by inductively coupled plasma double focusing sector field mass spec-trometry[J].J Anal At Spectrom,1999,14(9):1501-1504.
    [14]RODRGUEZ-FERNNDEZ J,MONTES-BAYN M,PEREIRO R,et al.Gas chromatography double focusing sector-field ICP-MS as an innova-tive tool for bad breath research[J].J Anal At Spectrom,2001,16(9):1051-1056.
    [15]MENEGARIO A A,GINE M F,BENDASSO-LLI J A,et al.Sulfur isotope ratio(34 S:32 S)measurements in plant material by inductively coupled plasma mass spectrometry[J].J Anal Atom Spectrom,1998,13:1065-1067.
    [16]CRADDOCK P R,ROUXEL O J,BALL L A,et al.Sulfur isotope measurement of sulfate and sulfide by high-resolution MC-ICP-MS[J].Chem Geol,2008,253(3/4):102-113.
    [17]SCHAUMLFFEL D,THOLEY A.Recent di-rections of electrospray mass spectrometry for el-emental speciation analysis[J].Anal Bioanal Chem,2011,400(6):1645-1652.
    [18]NARUKAWA T,KUROIWA T,CHIBA K.Me-chanism of sensitivity difference between trivalent inorganic As species[As(III)]and pentavalent species[As(V)]with inductively coupled plas-ma spectrometry[J].Talanta,2007,73(1):157-165.
    [19]黄志丁,王军,逯海,等.电感耦合等离子体质谱法测定硫时不同形态硫的影响[J].岩矿测试,2012,31(1):77-82.
    [20]DIVJAK B,GOESSLER W.Ion chromatograph-ic separation of sulfur-containing inorganic anions with an ICP-MS as element-specific detector[J].J Chromatogr A,1999,844(1/2):161-169.
    [21]范立民,寇贵德,侯飞龙.榆神低硫煤中硫含量特征及成因探讨[J].中国煤田地质,2003,15(2):12-13.
    [22]MAKISHIMA A,NAKAMURA E.Determina-tion of total sulfur at microgram per gram levels in geological materials by oxidation of sulfur into sulfate with in situ generation of bromine using i-sotope dilution high-resolution ICPMS[J].Anal Chem,2001,73(11):2547-2553.
    [23]GUILLONG M,LATKOCZY C,SEO J H,et al.Determination of sulfur in fluid inclusions by laser ablation ICP-MS[J].J Anal Atom Spectrom,2008,23(12):1581-1589.
    [24]SEO J H,GUILLONG M,HEINRICH C A.The role of sulfur in the formation of magmatic-hydrothermal copper-gold deposits[J].Earth Planet Sc Lett,2009,282(1/2/3/4):323-328.
    [25]SEO J H,GUILLONG M,AERTS M,et al.Microanalysis of S,Cl,and Br in fluid inclusions by LA-ICP-MS[J].Chem Geol,2011,284(1/2):35-44.
    [26]COPLEN T,BHLKE J,De BIEVRE P,et al.Isotope-abundance variations of selected ele-ments:(IUPAC technical report)[J].Pure Appl Chem,2002,74(10):1987-2017.
    [27]CAI C,LI H,QIN M,et al.Biogenic and petro-leum-related ore-forming processes in Dongsheng uranium deposit,NW China[J].Ore Geol Rev,2007,32(1/2):262-274.
    [28]BETTMER J,MONTES BAYON M,RUIZ EN-CINAR J,et al.The emerging role of ICP-MS in proteomic analysis[J].J Proteomics,2009,72(6):989-1005.
    [29]AEBERSOLD R,MANN M.Mass spectrome-try-based proteomics[J].Nature,2003,422(6928):198-207.
    [30]THOMAS W,MARTIN O,STEFAN W,et al.The role of the Kupferschiefer in the formation of hydrothermal base metal mineralization in the Spessart ore district,Germany:Insight from de-tailed sulfur isotope studies[J].Miner Deposita,2010,45(3):217-239.
    [31]OLIVIER R,WAYNE C S,WOLFGANG B,et al.Integrated Fe-and S-isotope study of seafloor hy-drothermal vents at East Pacific Rise9-10°N[J].Chemical Geology,2008,252(3/4):214-227.
    [32]SCHAUMLFFEL D.New ways in qualitative and quantitative protein analysis:Nano chroma-tography coupled to element mass spectrometry[J].J Trace Elem Med Bio,2007,21(S1):18-22.
    [33]BALKHI S E,POUPON J,TROCELLO J M,et al.Human plasma copper proteins speciation by size exclusion chromatography coupled to in-ductively coupled plasma mass spectrometry.so-lutions for columns calibration by sulfur detection[J].Anal Chem,2010,82(116):6904-6910.
    [34]HANN S,KOELLENSPERGER G,OBINGER C,et al.SEC-ICP-DRCMS and SEC-ICP-SFMS for determination of metal-sulfur ratios in metal-loproteins[J].J Anal Atom Spectrom,2004,19(1):74-79.
    [35]GINER M-S J,MORENO S F,HERRERO E P,et al.Evaluation of different analytical strategies for the quantification of sulfur-containing biomol-ecules by HPLC-ICP-MS:Application to the characterisation of 34 S-labelled yeast[J].J Anal At Spectrom,2010,25(7):989-997.
    [36]YEH C-F,JIANG S-J,HSI T S.Determination of sulfur-containing amino acids by capillary elec-trophoresis dynamic reaction cell inductively cou-pled plasma mass spectrometry[J].Anal Chim Acta,2004,502(1):57-63.
    [37]RAPPEL C,SCHAUMLOEFFEL D.The role of sulfur and sulfur isotope dilution analysis in quantitative protein analysis[J].Anal Bioanal Chem,2008,390(2):605-615.
    [38]SCHAUMLOFFEL D,GIUSTI P,PREUD’HO-MME H,et al.Precolumn isotope dilution analy-sis in nanoHPLC-ICPMS for absolute quantifica-tion of sulfur-containing peptides[J].Anal Chem,2007,79(7):2859-2868.
    [39]WANG M,FENG W,LU W,et al.Quantita-tive analysis of proteins via sulfur determination by HPLC coupled to isotope dilution ICPMS with a hexapole collision cell[J].Anal Chem,2007,79(23):9128-9134.
    [40]CAUMETTE G,LIENEMANN C P,MERDRI-GNAC I,et al.Element speciation analysis ofpetroleum and related materials[J].J Anal At Spectrom,2009,24(3):263-276.
    [41]EVANS P,WOLFF-BRICHE C,FAIRMAN B.High accuracy analysis of low level sulfur in diesel fuel by isotope dilution high resolution ICP-MS,using silicon for mass bias correction of nat-ural isotope ratios[J].J Anal Atom Spectrom,2001,16(9):964-969.
    [42]HEILMANN J,BOULYGA S F,HEUMANN K G.Accurate determination of sulfur in gasoline and related fuel samples using isotope dilution ICP-MS with direct sample injection and micro-wave-assisted digestion[J].Anal Bioanal Chem,2004,380(2):190-197.
    [43]BOULYGA S F,HEILMANN J,HEUMANN K G.Isotope dilution ICP-MS with laser-assisted sample introduction for direct determination of sulfur in petroleum products[J].Anal Bioanal Chem,2005,382(8):1808-1814.
    [44]HEILMANN J,HEUMANN K G.Development of a species-unspecific isotope dilution GC-ICPMS method for possible routine quantification of sul-fur species in petroleum products[J].Anal Chem,2008,80(6):1952-1961.
    [45]HEILMANN J,HEUMANN K G.Development of a species-specific isotope dilution GC-ICP-MS method for the determination of thiophene deri-vates in petroleum products[J].Anal Bioanal Chem,2008,390(2):643-653.
    [46]BOUYSSIERE B,LEONHARD P,FROCK D,et al.Investigation of the sulfur speciation in pe-troleum products by capillary gas chromatogra-phy with ICP-collision cell-MS detection[J].J Anal At Spectrom,2004,19(5):700-702.
    [47]SABLS,COTTENCEAU G.Current knowl-edge of soft cheeses flavor and related compounds[J].J Agr Food Chem,1999,47(12):4825-4836.
    [48]LANDAUD S,HELINCK S,BONNARME P.Formation of volatile sulfur compounds and me-tabolism of methionine and other sulfur com-pounds in fermented food[J].Applied microbiol-ogy and biotechnology,2008,77(6):1191-1205.
    [49]RICARDO L′OPEZ,CRISTINA L A,CACHO J,et al.Quantitative determination of wine high-ly volatile sulfur compounds by using automated headspace solid-phase microextraction and gas chromatography-pulsed flame photometric detec-tion Critical study and optimization of a new pro-cedure[J].Journal of Chromatography A,2007,1143(1/2):8-15.
    [50]YU F,MICHAEL C,QIAN.Sensitive quantifi-cation of sulfur compounds in wine by headspace solid-phase microextraction technique[J].Journal of Chromatography A,2005,1080(2):177-185.
    [51]GINER MARTI NEZ-SIERRA J,SANTAMAR-IA-FERNANDEZ R,HEARN R,et al.Devel-opment of a direct procedure for the measurement of sulfur isotope variability in beers by MC-ICP-MS[J].J Agr Food Chem,2010,58(7):4043-4050.