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在“
Elsevier电子期刊
”中,
命中:
56
条,耗时:0.0639768 秒
1.
Enhancing analysis throughput, sensitivity and specificity in LC/ESI-MS/MS assay of plasma 25-hydroxyvitamin D
3
by derivatization with triplex 4-(4-dimethylaminophenyl)-1,2,4-triazoline-3,5-dione (DAPTAD) isotopologues
作者:
Shoujiro Ogawa
a
;
Hiroki Kittaka
a
;
Akiho Nakata
a
;
Kenji Komatsu
b
;
Takahiro Sugiura
b
;
Mamoru Satoh
c
;
Fumio Nomura
c
;
Tatsuya Higashi
a
;
higashi@rs.tus.ac.jp
关键词:
LC/ESI&
ndash
;
MS/MS
;
Derivatization
;
Isotopologue
;
Analysis throughput
;
Vitamin D
刊名:Journal of Pharmaceutical and Biomedical Analysis
出版年:2017
2.
Identification, synthesis and structural characterization of process related and degradation impurities of acrivastine and validation of HPLC method
作者:
Ajay Kumar
b
;
Subba Rao Devineni
a
;
Shailender Kumar Dubey
a
;
Pradeep Kumar
b
;
Vishal Srivastava
b
;
Girish Ambulgekar
a
;
Mohit Jain
b
;
Dharmendra Kumar Gupta
a
;
Gurmeet Singh
b
;
Rajesh Kumar
b
;
S.G. Hiriyanna
b
;
Pramod Kumar
a
;
pramodkumar@microlabs.in
关键词:
Acrivastine
;
Forced degradation
;
Impurities
;
Identification
;
Characterization
;
Method validation
刊名:Journal of Pharmaceutical and Biomedical Analysis
出版年:2017
3.
Methods for differential and quantitative analyses of brain neurosteroid levels by LC/MS/MS with ESI-enhancing and isotope-coded derivatization
作者:
Tatsuya Higashi
;
higashi@rs.tus.ac.jp" class="auth_mail" title="E-mail the corresponding author
;
Naoto Aiba
;
Tomoya Tanaka
;
Kazumi Yoshizawa
;
Shoujiro Ogawa
关键词:
Neurosteroid
;
Rat brain
;
LC/ESI&
ndash
;
MS/MS
;
Isotope-coded derivatization
;
Antipsychotic drug
刊名:Journal of Pharmaceutical and Biomedical Analysis
出版年:2016
4.
Four process-related potential new impurities in ticagrelor: Identification, isolation, characterization using HPLC, LC/ESI-MS
n
, NMR and their synthesis
作者:
Neeraj Kumar
a
;
Subba Rao Devineni
a
;
Prasad Reddy Gajjala
a
;
Dharmendra Kumar Gupta
a
;
Sandesh Bhat
a
;
Rajesh Kumar
b
;
Shailendra Kumar Dubey
a
;
Pramod Kumar
a
;
pramodkumar@microlabs.in" class="auth_mail" title="E-mail the corresponding author
关键词:
Ticagrelor
;
Impurities
;
Identification
;
Isolation
;
LC&
ndash
;
ESI/MS
;
NMR
刊名:Journal of Pharmaceutical and Biomedical Analysis
出版年:2016
5.
Chemical derivatization for enhancing sensitivity during LC/ESI-MS/MS quantification of steroids in biological samples: a review
作者:
Tatsuya Higashi
;
higashi@rs.tus.ac.jp" class="auth_mail" title="E-mail the corresponding author
;
Shoujiro Ogawa
关键词:1 ;
25(OH)2D2
;
1α
;
25-dihydroxyvitamin D2
;
1
;
25(OH)2D3
;
1α
;
25-dihydroxyvitamin D3
;
17(OH)P4
;
17α-hydroxyprogesterone
;
17(OH)P5
;
17α-hydroxypregnenolone
;
24
;
25(OH)2D3
;
24R
;
25-dihydroxyvitamin D3
;
25(OH)D2
;
25-hydroxyvitamin D2
;
25(OH)D3
;
25-hydroxyvitamin D3
;
3α
;
5α-Adiol
;
3α
;
5α-androstanediol
;
4
;
25(OH)2D3
;
4β
;
25-dihydroxyvitamin D3
;
AD
;
androstenedione
;
AP
;
allopregnanolone
;
APA
;
aldosterone-producing adenoma
;
APCI
;
atmospheric pressure chemical ionization
;
BPH
;
benign prostate hyperplasia
;
CAH
;
con
刊名:Journal of Steroid Biochemistry and Molecular Biology
出版年:2016
6.
9,10-Phenanthrenequinone as a mass-tagging reagent for ultra-sensitive liquid chromatography-tandem mass spectrometry assay of aliphatic aldehydes in human serum
作者:
Mahmoud El-Maghrabey
a
;
b
;
Naoya Kishikawa
a
;
Naotaka Kuroda
a
;
n-kuro@nagasaki-u.ac.jp" class="auth_mail" title="E-mail the corresponding author
关键词:9 ;
10-Phenanthrenequinone
;
LC/ESI&
ndash
;
MS/MS
;
Aliphatic aldehydes
;
Human serum
刊名:Journal of Chromatography A
出版年:2016
7.
Identification, isolation and characterization of potential process-related impurity and its degradation product in vildagliptin
作者:
Neeraj Kumar
a
;
Subba Rao Devineni
a
;
Gurmeet Singh
b
;
A. Kadirappa
a
;
Shailendra Kumar Dubey
a
;
Pramod Kumar
a
;
pramodkumar@microlabs.in" class="auth_mail" title="E-mail the corresponding author
关键词:
Vildagliptin
;
Impurity degradation
;
Identification
;
Isolation
;
LC/ESI&
ndash
;
MSn
;
NMR
刊名:Journal of Pharmaceutical and Biomedical Analysis
出版年:2016
8.
Development and validation of LC-MS methods for peptaibol quantification in fungal extracts according to their lengths
作者:
Anne-Isaline Van Bohemen
a
;
Aurore Zalouk-Vergnoux
a
;
aurore.zalouk-vergnoux@univ-nantes.fr" class="auth_mail" title="E-mail the corresponding author
;
Laurence Poirier
a
;
Nam Ngoc Phuong
a
;
Nicolas Inguimbert
b
;
Khoubaib Ben Haj Salah
b
;
Nicolas Ruiz
a
;
Yves Franç
;
ois Pouchus
a
关键词:
Trichoderma sp
;
Peptaibols
;
LC/ESI-IT-MS
;
Quantification
;
Validation
;
Biocontrol
刊名:Journal of Chromatography B, Analytical Technologies in the Biomedical and Life Sciences
出版年:2016
9.
LC and LC-MS study for simultaneous determination of tramadol hydrochloride and ketorolac tromethamine in bulk and formulation with their major degradation products
作者:
Vrushali S. Tambe
a
;
d
;
vrushali.tambe@rediffmail.com" class="auth_mail" title="E-mail the corresponding author
;
M.N. Deodhar
b
;
d
;
Vijayalakshmi Prakya
c
;
d
关键词:
Tramadol
;
Ketorolac
;
LC&
ndash
;
MS
;
Stability
刊名:Bulletin of Faculty of Pharmacy, Cairo University
出版年:2016
10.
A lipidomic analysis approach in patients undergoing lipoprotein apheresis
作者:
C. Schmö
;
cker
a
;
b
;
U. Kassner
a
;
S. Kiesler
a
;
M. Bismarck
a
;
M. Rothe
c
;
E. Steinhagen-Thiessen
a
;
K.H. Weylandt
a
;
d
;
karsten.weylandt@charite.de" class="auth_mail" title="E-mail the corresponding author
关键词:
Lipid apheresis
;
Hyperlipoproteinaemia
;
Gas chromatography
;
Oxylipine
;
Lipidomic
;
LC/ESI-MS/MS
;
PUFA
刊名:Atherosclerosis
出版年:2016
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